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GC/MS analysis results for sample AD22552, Sept 2001

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Laboratory report documenting GC/MS analysis of sample AD22552 conducted on September 27, 2001, identifying unknown compounds.

NYC-WTC_000087068–000087087

Folder label: “508 Scan 9/18/01 9/27/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2601\22552.D Vial: 6 Acq On : 26 Sep 2001 4:15 pm Operator: GALOS Sample : GC/MS unknown Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library ; C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Heptadecane Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 31.92 1.26 ng/uL 92701 Chrysene-dl2 33.31 Hit# of 5 Tentative ID MW MolForm CAS# Qual y Heptadecane 240 C17H36 000629-78-7 83 ■2 Nonane, 2,5-dimethyl- 156 C11H24 017302-27-1 50 3 Decane, 2,2,8-trimethyl- 184 C13H28 062238-01-1 45 4 Hexadecane 226 C16H34 000544-76-3 39 Abundance Scan 2954 (31.924 min): 22552.D (-) m/z 57.10 100.00% 5/ 43 71

5000 85 A I ' ' ‘ ' I 99 31.60 31.80 32.00 32.20 ,1 m/z 43.10 76.52% I ' ' ' ' I ' n/z-> 20 40I 60 80 100 120 140 160 180 200 220 240 Abundance #71191: Heptadecane 57 43

71 ........ t\\ \....... 5000 85 31.60 31.80 32,00 32.20 m/z7170567.39% II Tl/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #11616: Nonane, 2,5-dimethyl- 57 43 31,60 31.80 32.00 32.20 m/z 85.05 38.92% 5000 85 n I I 99

nZz-> 20 XJ 40 (60 80 , j| , 112 141 .................. 100 120 140 160 180 200 220 240 Abundance #19012: Decane, 2,2,8-trimethyl- 57 31.60 31.80 32.00 32.20 m/z41.10 32.99%

5000

71 ftc 2/ 42 ' , ,! , Vn ^27 , , , , 169 ..........fY.. 20 40 60 80 100 120 140 160 180 200 220 240 31.60 31.80 32.00 32.20

22552.D NP072501.M Mon Oct 01 13:03:21 2001 Page 7

NYC-WTC_000087083

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