GC/MS analysis results for sample AD22552, Sept 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2601\22552.D Vial: 6 Acq On : 26 Sep 2001 4:15 pm Operator: GALOS Sample : GC/MS unknown Inst : GC/MS Ins Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Hexane, 2,3,4-trimethyl- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 30.89 0.40 ng/uL 29556 Chrysene-dl2 - 33.31 Hit# of Tentative ID MW MolForm CAS# Qual 1 Hexane, 2,3,4-trimethyl- 128 C9H20 000921-47-1 33 2 Pentane, 2-bromo- 150 C5HllBr 000107-81-3 9 3 Pj/opanoic acid, 2-methyl-, 2-ethyl- 286 C16H30O4 074367-30-9 9 4 X^xane, 3-ethyl-C8H18 000619-99-8 9 <\bqfidance Scan 2841 (30.888 min): 22552. D (-) m/z 57.10 100.00% 5|7 43 71 5000 85

30.60 30.80 31.00 31.20 m/z 43.10 73.39% Tl^-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #5147: Hexane, 2,3,4-trimethyl- 43

5000 57 71 85 30.60 30.80 31.00 31.20 27 m/z 71705 60.48% 128 1-p-m-jT I'''' I'''' I'''' r I ' ' ’ ’ I ! ' ' ' I n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66675; Pentane, 2-bromo- 43 71 30.60 30.80 31.00 31.20 5000- 27 m/z 85.15 35.01% 55

....P........ T-pT-T-r-I^TTrp-T-T-rp- 107 123 150 f' ' ' ' I ' ' ' * I ' ' ' ' I ' ' ' ’ 1 ■nyz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #40504: Propanoic acid, 2-methyl-, 2-ethyl-1-propyl-1,3-pro 40 30.60 30.80 31.00 31.20 m/z 41710 31.20% 71 A 5000 55

81 89 110 127 143 155 ' I ' -T-j-T-TT-rT-r-r-rry-r-rTT-p-TTT-p-^^ n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 30.60 30.80 31.00 31.20

22552.D NP072501.M Mon Oct 01 13:03:20 2001 Page 6

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