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GCMS analysis results for sample AD24238, Nov 5 2001

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Laboratory report documenting GCMS analysis of sample AD24238 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068101–000068116

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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Scanned page image, NYC-WTC_000068111
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3101\24237.D Vial: 4 Acq On : 31 Oct 2001 7:02 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.56 0.46 ug/1 63394 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexanoy 102 C6H14O 000623-37-0 74 2 3-Penta/ol 88 C5H12O 000584-02-1 38 3 3-Pen^nol, 2-methyl- 102 C6H14O 000565-67-3 36 4 Silape, trimethyl- 74 C3H10Si 000993-07-7 32 Abundance Z Scan 165 (6.555 min): 24237.D (-) m/z 59.05 100.00% 56

5000 73 43 6.20 6.40 ft. 6.60 6.80 .... 85 ' I ‘ r‘ * I ‘ ‘ ‘ I ‘ ‘ 1 m/^ 55.00 81.99% Tife-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63529:3-Hexanol 56

31 5000 73 6.20 6.40 6.60 6.80 m/z 73.00 41.30% 44 rT+44^ 44................. 102 ■ ' I ‘ ‘ ■ I ■ ‘ ■ ■ I Tife-> 10 20 30 40 50 60 70 80 90 100 110 \bunclance #62943; 3-Pentanol

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31 620 6.40 6.60 6.80 5000 m/z 43.00 22.32% 41

I'l ■ • > ■ I ■ ■ ■ > I I ‘ * I I • • > ■ I > ■ • ■ I TiZz-> 10 20 30 40 50 I60 70 80 90 100 110 Abundance #1781:3-PentanoI. 2-methyi- 56 'e.^''aTO' RTO ■m/z 41.05 20.57% 5000 31 73

45 15 I I I ' ‘ ' I ' ■-r Tlfe-> 10 20 30 40 50 60 70 80 90 100 110

24237.D NP103001.M Fri Nov 02 11:57:38 2001 Page 3

NYC-WTC_0000681 11

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NYC-WTC_000068111Source: NYC Law Department, mirrored locally

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