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GCMS analysis results for sample AD24238, Nov 5 2001

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Laboratory report documenting GCMS analysis of sample AD24238 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068101–000068116

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT3101\24237.D Vial: 4 Acq On : 31 Oct 2001 7:02 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise ; Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Pentanol, 4-methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.67 0.55 ug/1 76090 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 83 2 2-Hexanol 102 C6H14O 000626-93-7 78 3 2-Octanol, (R)- 130 C8H18O 005978-70-1 72 4 2-Octanol, (S) - 130 C8H18O 006169-06-8 72 Abundance Scan 178 (6.675 min): 24237.D(-) m/z 44.95 100.00% 4fe

5000

69 6.40 6.60 6.80 7.00 98 Tlfe-> 10 " '30' ' I ' I ' ‘ ‘ 1 ' ' ‘ ' I ' ' ' ' I ' m/z 41.05 16.20% 40 50 60 70 80 90 100 110 120 Abundance

jWL #1773:2-Pentanol, 4-methyl-

5000 6.40 6.60 6.80 7.00 69 nTz 69700 14.83% 27 57 ..... ,. -,.,^4 nfe-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #63582:2-Hexanol 45

6.40 6.60 6.80 7.00 5000 m/z 42.95 11.26%

■nfe-> 10 Abundance 19 27 I . ’ I ' ' ' ' 1 • 20 30 40

45 57 I ' ''I'' I 50 60 70 69 I 80 #5523:2-Octanol, (R). 87 ■ I'I■'I•■■■I' ■ ■ ■ 1 ‘ ‘ 90 100 110 • 1 • 120 J/6.40 I. m/F 43.95 6.60 6.80 7.00 8.86% =f

5000

27 I • ■ • • I ■ • 1 ■ ■ • • I I I ' ' I ■ ' I ‘ ‘ ■ ''I • • ' ■ I ‘ ■ I ' ‘ 115 ‘ I ‘ I ■ • ‘ ‘ I ‘ nZz-> 10 20 30 40 50 60 70 80 90 100 110 120 6.40 6.60 6.80 7.00

24237.D NP103001.M Fri Nov 02 11:57:41 2001 Page 4

NYC-WTC_000068112

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NYC-WTC_000068112Source: NYC Law Department, mirrored locally

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