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GCMS analysis results for sample AD24238, Nov 5 2001

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Laboratory report documenting GCMS analysis of sample AD24238 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068101–000068116

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3101\24237.D Vial: 4 Acq On : 31 Oct 2001 7:02 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 2.40 ug/1 332297 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 fentative ID MW MolForra CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 39 2 Hydrazin^ 1,1-bis(1-methylethyl)- 116 C6H16N2 000921-14-2 28 3 3-Hydro^-2-pentanone 102 C5H10O2 003142-66-3 9 4 Morphol/ine, 4-methyl-______________ 101 C5H11NO 000109-02-4 9 Wiundanoe Scan 289 (7.^4 min): 24237.D (-) m/z 42.9^ 100.05% 43

59 5000 101 . 71 83 j1 L 207 l'q"+ j...1,1,.,, m/z 59705 52.93% 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #3245:2-Pentanone, 4-hydroxy-4-m8thyl- 4)3

5000 59 7.40 7.60 7.80 8.00 m/z 100.95 24.46%

_L. 31 I 101 i 11 > I I I I i H i I . I I I I . 1 I . I 11 I. I 11 iTp i I > I .. . I I I . Il I I H I I . I 11 I ■ I I > 11. I I I < < I > I I ( I. I

vk-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Mxjndance #3324: Hydrazine, 1,1-bis(1-niethylethyt)- 5)9

7.40 7.60 7.80 8.00 5000 101 m/z 58705 18.71% 42 27 116 PTttptI+tttttLtttU 73 84 I " "I "nI Tife-> 10 2330 40 50 60 70 80 90 100110120130140150160170180190ZX)210 \bundance #1691:3-Hydroxy-2-pentanone 31 7.40 7.60 7.80 8.00 m/z 41.05 8.07% 5000 45 15 ,__ 73 84 102 _________ T 11... 11.,, I 111,1.1 U I I... 11.1111,, 11,. ,. I ..,, I,. ,, I., ., I,... I.... 11, , 1 I. I ., I I*' ”1 ““I ““I TiZz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 7.40 7.60 7.80 8.00

24237.D NP103001.M Fri Nov 02 11:57:43 2001 Page 5

NYC-WTC_000068113

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NYC-WTC_000068113Source: NYC Law Department, mirrored locally

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