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GCMS results log, sample AD27007, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD27007 completed on December 11, 2001.

NYC-WTC_000032503–000032519

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\27007.D Vial: 22 Acq On 7 Dec 2001 5:16 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Hexadecane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

33.75 0.77 ng/uL 225165 Chrysene-dl2 33.19

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecane 226 C16H34 000544-76-3 <93. 2 Hexatriacontane 507 C36H74 000630-06-8 90 3 Dotriacontane 451 C32H66 000544-85-4 87 4 Hexatriacontane_____________________ 507 C36H74 000630-06-8 87 Abundance Scan 3152 (33.746 min): 27007.D (-) m/z 57.10 100.00% 57

5000 - 85 -A f TT

miz-> XU 113 50 100 150 200 226 250 300 350 400 450 33.40 33.60 33.80 34 00 m/ z 4 3.10 64.97% Abundance #70790: Hexadecane i 7

/ 5000 i ■ 1 1 ■ i • 85 33.40 33.60 33.80 34.00 m/ Z 71." 59.54% 226 ' ' 1 r-I_113 ---I_141 169- --------- m/z-> 50 100 150 200 250 300 350 400 450 Abundance #74636: Hexatriacontane 57 TT 33.40 33.60 33.80 34.00 5000 85 m/ z 85.05 39.25%

I IL II1,'!3. 141 169 197 miz-> 50 100 150 200 250 300 350 400 450 Abundance #74491: Dotriacontane TEEEL IT 57 33.40 33.60 33.80 34.00 m/ Z 55.10^ 26.32% 5000 85

I 1’1141, 196 281 422 450 ' I-r-T—j—r — TT m/z-> 50 100 150 200 250 300 350 400 450 33.40 33.60 33.80 34.00

27007.D NP112701.M Tue Dec 11 14:57:04 2001 Page 7

NYC-WTC_000032517

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NYC-WTC_000032517Source: NYC Law Department, mirrored locally

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