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GCMS results log, sample AD27007, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD27007 completed on December 11, 2001.

NYC-WTC_000032503–000032519

Folder label: “GCMS X 11/8/01 A 12/7/01

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Scanned page image, NYC-WTC_000032518
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\27007.D Vial: 22 Acq On 7 Dec 2001 5:16 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 8 Pentatriacontane Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

34.66 0.41 ng/uL 118769 Chrysene-dl2 33.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentatriacontane 493 C35H72 000630-07-9 io) 2 Dotriacontane 451 C32H66 000544-85-4 907 3 Octacosane 394 C28H58 000630-02-4 83 4 Hexatriacontane 507 C36H74 _______ 000630-06-8 78 'Abundance Scan 3252 (34.663 min): 27007.D (-) m/ z 57.10 100.00%] 57

5000 85 ——14 | 34.40 34.60 34.80 35.00 207 m/z 43 . 0 65.78% m/z-> 50 WO 150 200 250 300 350 400 450 Abundance #58743: Pentatriacontane 57

5000 —A—....... ...... .................. 85 34.40 34.60 34.80 35.00 m/z " 58.57% [| 113,141 , 169 197 225 T ' i 'm/z-> 50 100 150 200 250 300 350 400 450 Abundance #74491: Dotriacontane 57 T 34.40 34.60 34.80 35.00 5000 85 m/ z 85.05 42.92%

113 141 I i 196 281 422 450 k‘T" m/z-> 50 100 150 200 250 300 350 400 450 Abundance #74211: Octacosane ■ i ' ■ 43 34.40 34.60 34.80 35.00 m/z 55.10 26.24% 71 5000

99 , Il , 127 155 183 211 364 ■ ■ I ' ■ A 1 ' 1 1 ' m/z-> 50 100 150 200 250 300 350 400 450 34.40 34.60 34.80 35.00

27007.D NP112701.M Tue Dec 11 14:57:07 2001 Page 8

NYC-WTC_000032518

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NYC-WTC_000032518Source: NYC Law Department, mirrored locally

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