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GCMS analysis results for sample AD26006, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26006 conducted on December 19-20, 2001.

NYC-WTC_000030836–000030853

Folder label: “GCMS SCAN X 10/31/01 AN 11/21/01

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Scanned page image, NYC-WTC_000030849
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\26006A.D Vial: 4 Acq On : 20 Dec 2001 9:36 am Operator: GALOS Sample : gc/ms unknown 10/31 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Pentatriacontane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

33.71 0.62 ng/uL 201961 Chrysene-dl2 33.17

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentatriacontane 2 Nonacosane 493 408 C35H72 C29H60 000630-07-9 000630-03-5 87 (9) 3 Hexatriacontane 507 C36H74 000630-06-8 83 4 Octadecane 254 C18H38 000593-45-3 83 Abundance Scan 3148 (33.713 min): 26006A.D (-) m/Z 57.10 100.00%] 57

5000 85 J m/z~> Abundance a 208I ............................. — 226 281 । < l।।।q ii ii 111111111 r|'ri 111 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 #58743: Pentatriacontane 33.40 33.60 33.80 34.00 m/z 43.10 67.95%

i 57 i

5000 85 33.40 33.60 33.80 34.00 m/z 71.10 60.85% 1 113 141 i ■ 1 169 197 225 I i" " I'"' i" " i' r .1 i j)... I.... I.... I i1 " ‘ I ■ 1 * • i I ... . | ... .-|. 11 I | |V|

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #54526: Nonacosane 43 I . . । —P . T F N 71 33.40 33.60 33.80 34.00 5000 m/z 85.15 41.05% -

। 99 127 211 239 379 408 i T’I 11... II i" " r TTITTTTTTTMTLTTTTUITpgmmn m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #74636: Hexatriacontane -AAA4M4AA —AM—A4 AAAA i 57 33.40 33.60 33.80 34.00 I I m/z 41.10 26.50% 5000 85

v WW~ WV/w I I ll 113,169 197 "11 ' TTTITTTTTTTTTICTETTIITTTpgjun 1 1 ' 1 1 I miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 33.40 33.60 33.80 34.00

26006A.D NP112701.M Thu Dec 20 10:39:55 2001 Page 6

NYC-WTC_000030849

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NYC-WTC_000030849Source: NYC Law Department, mirrored locally

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