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GCMS analysis results for sample AD26006, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26006 conducted on December 19-20, 2001.

NYC-WTC_000030836–000030853

Folder label: “GCMS SCAN X 10/31/01 AN 11/21/01

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Scanned page image, NYC-WTC_000030848
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\26006A.D Vial: 4 Acq On : 20 Dec 2001 9:36 am Operator: GALOS Sample : gc/ms unknown 10/31 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Triacontane Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

32.77 0.51 ng/uL 165262 Chrysene-dl2 33.17

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Triacontane 422 C30H62 000638-68-6 1 2 Tritetracontane 605 C43H88 007098-21-7 91 3 Hexatriacontane 507 C36H74 000630-06-8 90 4 Nonadecane 268 C19H40 000629-92-5 86 'Abundance Scan 3045 (32.768 min): 26006A.D (-) m/z 57.10 100.00% 57

5000 85

1 i 1 ' ‘I1

— 141141—— 32.40 32.60 32.80 33.00 33.20

mlz-> Abundance 50 100 150 200 250 300 350 400 #55461: Triacontane 450 500 550 600 m/z 43. ¥ 71.38%

43

71 i 5000 ‘d TT 32.40 32.60 32.80 33.00 33.20 m/z 71.05 58.64% . 99 .07 45.......... 239267 - —379 422 'm/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #60913 Tritetracontane 57

32.40 32.60 32.80 33.00 33.20 5000 85 m/z 85.15 42.79% -

1141— ...................................... 463 491 519 547 576604 m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #74636: Hexatriacontane -- — 444 57 32.40 32.60 32.80 33.00 33.20 m/z 41.1 0 28.46% 5000 85 II I WAA/ I vANNw i 1 1 I' 11l3141 169197 ............. .... — miz-> 50 100 150 200 250 300 350 400 450 500 550 600 32.40 32.60 32.80 33.00 33.20

26006A.D NP112701.M Thu Dec 20 10:39:53 2001 Page 5

NYC-WTC_000030848

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