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GC/MS analysis results for sample AD23606, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23606 conducted on October 19, 2001.

NYC-WTC_000088961–000088985

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088975
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : “C:\HPCHEM\l\DATA\OCTi601\23606.D Vial: 13 Acq On : 17 Oct 2001 1:59 am Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Triacontane Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 30.70 1.03 ug/1 124523 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Triacontane 422 C30H62 000638-68-6 91s 2 Pentacosane 352 C25H52 000629-99-2 91 3 Heptadecane 240 C17H36 000629-78-7 91" 4 Tetracosane ____________________ 338 C24H50 000646-31-1 90 Abundance Scan 2795 (30.701 min): 23606.D (-) m/z 57700 100.00% 57

5000 85

Tt-rr-r 30.40 30.60 30.80 31.00 3! JTrtTpVrTpT'TTyTTTrl’TTTYpTTTJTTTTy^ I ■ I.. 11... 1, 11 . 11 m/z 71.00 73.55% tVz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #55461: Triacontane 4)3

71 253 ,, ............ 30.40 30.60 30.80 31.00

tVz-> Aibundance uw 99 127 1Uh-../.. 239 267 ‘' 1"' I'' I" " I" " I 40 60 80 100120140160180 200220 240260280 300320 340360380 400420 #73718: Pentacosane 379 422 m/z 4^705 72.95%

43 ? , p. . I- r I . r . f. 71 30.40 30.60 30.80 31.00 5000 m/z 85.05 50.25%

Ti/z-> Vrr,Vrr r tu 99 ,127 155 183 211 T*ryTVTTfTTT^qTT-rTpT-TT[TTTTpTTrpTTTpTTTyrTTrpTTTJTTT^^ 40 60 80 100120140160180200220 240260280 300320 340360380400420 Abundance #71193: Heptadecane I ' 57 30.40 30.60 30.80 31.00 m/z - 41.00.- 2.7-..19.%

5000 85

169 210 240 I "."I nT -p-m-pTrn-f n/z-> 40 60 80 100120140160180 200220 240260 280 300320 340360 380 400 420 30.40 30.60 30.80 31.00

23606.D NP091101.M Thu Oct 18 10:35:55 2001 Page 8

NYC-WTC_000088975

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NYC-WTC_000088975Source: NYC Law Department, mirrored locally

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