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GC/MS analysis results for sample AD23606, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23606 conducted on October 19, 2001.

NYC-WTC_000088961–000088985

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088976
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23606.D Vial: 13 Acq On : 17 Oct 2001 1:59 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Octadecanoic acid, 2-methylpro Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. -------------:-----------------------------i____

31.65 2.20 ug/1 265431 Chrysene-dl2 33.12 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 OctadecMloic acid, 2-methylpropyl e 340 C22H44O2 000646-13-9 70 2 Butyl etradecanoate (myristate) 284 C18H36O2 000000-00-0 64 3 Oxi^(ne, 2,3-bis(l-methylethyl)-, t 128 C8H16O ’ 054644-32-5 '32 4 OcXadecanoic acid, butyl ester 340 C22H44O2 000123-95-5 28 ^bundance Scan 2898 (31.646 min): 23606.D (-) m/z 56.00 100.00% 53

5000 4' 73 129 285

TTfe-> 40 '' I L,. 60 80 VlI, , [ .^^^57171^^1^1^241 100 120 140 160 180 200 220 240 260 280 300 320 340 I 340 m/z f ' ' ' 'I 31.40 31.60 31.80 32.00 57.00 52.42% Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 57

5000 31.40 31.60 31.80 32.00 285 m/z 43.05 41.50% 267 J I i.7mT I I I j 1 r I I I r I . I I . I 241 I I I I I 1 . I rn I I I I 1 I i' I I I I I 11 i I I Fl I . I 340 A nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320'340 Abundance #40186: Butyl tetradecanoate (myristate) —55

31.40 31.60 31.80 32.00 5000 m/z 41.05 35.62% 229 211 284 (I J •J"'I " I " " I' ’ I' " ' I H .. I • r.. I .-I I. I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #5067: Oxirane, 2,3-bis(1-methylethyl)-, trans- 55 31:40^ 31:60-31-.80-32.00 — -41- m/z 73.00 31.22%

5000

113128 I'''' I''I'''' I' ‘ r' ' I''' H ■nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23606.D NP091101.M Thu Oct 18 10:35:57 2001 Page 9

NYC-WTC_000088976

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NYC-WTC_000088976Source: NYC Law Department, mirrored locally

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