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GC/MS analysis results for sample AD23606, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23606 conducted on October 19, 2001.

NYC-WTC_000088961–000088985

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088977
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23606 .D Vial: 13 Acq On : 17 Oct 2001 1:59 am Operator: 2 09 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P ,

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Tetracosane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 31.74 2.06 ug/1 248671 Chrysene-dl2 33.12 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

/1 /Tetracosane 338 C24H50 000646-31-1 91-. Tricosane 324 C23H48 000638-67-5 87' 3 Octadecane 254 C18H38 . 000593-45-3 87 4 Heptadecane 240 C17H36 000629-78-7.87 Abundance Scan 2908 (31.738 min): 23606.D (-) m/z 57.00 100.00% 57 I . ■

43 71

5000 85

TiZz-> Abundance 40 ML/ u60 99 I I T. 1 I I . 1T I I I . 1 . f I . ,1 I , r 1 .1 ■., .. I . . . . I . , ., I , , , I I . . , , I , ., , I , I , I I , I, , I I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #73543: Tetracosane V 31.40 31.60 31.80 32.00 m/z 71.00 69.48%

43 57 71

5000 85 ................. 31.40 31.60 31.80 32.00 m/z 43.05 67.73% 155169183197 294 338 '' I' r 11 11 .1TI fI I I Iyt|11 I I' ■I "• I ' ' ' M ’ I ' • ' ' I I ' ' ' 'I •n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #46165: Tricosane _4l3_.57___

71 31.40 31,60 31.80 32.00 5000 m/z 85.05 49.72% 85

J T 155169183197211 253 297 324 TTpnnnyTTTTpTnTyTTTTp-TTTpTT-TpT-TTyrTTTTTTTTpTTnq-rTTTpTnTyT^^ Tife-> Abundance 40

43 57 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #71560: Octadecane XL 31.40 31.60 31.80 32.00 u' m/.-z-^4L...OO 28.35%

5000 71 85 k*

Tl/Z-> 40 60 169183197 80 100 120 140 160 180 200 220 240 260 280 300 320 340 254 ' ■ ’ I ' ' •' I' ' ‘ ' I ' '■’T' ' I M 31.40 31.60 31.80 32.00 ■n

23606.D NP091101.M Thu Oct 18 10:35:59 2001 Page 16

NYC-WTC_000088977

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NYC-WTC_000088977Source: NYC Law Department, mirrored locally

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