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GCMS analysis results for sample AD26006, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26006 conducted on December 19-20, 2001.

NYC-WTC_000030836–000030853

Folder label: “GCMS SCAN X 10/31/01 AN 11/21/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\26006A.D Vial: 4 Acq On : 20 Dec 2001 9:36 am Operator: GALOS Sample : gc/ms unknown 10/31 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 7 Heptacosane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

34.63 0.47 ng/uL 152842 Chrysene-dl2 33.17

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heptacosane 380 C27H56 000593-49-7 83 2 Nonadecane 268 C19H40 000629-92-5 83 3 Hexatriacontane 507 C36H74 000630-06-8 80 4 Pentacosane 352 C25H52 000629-99-2 80 Abundance Scan 3248 (34.630 min): 26006A.D (-) m/ z 57.10 100.00% 57

5000 85 i I

miz-> ‘T 50 nll__ +299-281 ........— 100 150 200 250 300 350 400 450 500 34.20 34.40 34.60 34.80 35.00 m/z 43.10 63.92% Abundance #52248: Heptacosane 57

5000 85 34.20 34.40 34.60 34.80 35.00 m/ z 71.15 54.63% 1 LL 1113.141,169 196 224 281 324 380 m/z-> 50 100 150 200 250 300 350 400 450 500 'Abundance #37469: Nonadecane 57 T 34.20 34.40 34.60 34.80 35.00 85 5000 m/z 85.15 38.47%-

1 1.113 ....... 183 ......... 268 ............. miz-> 50 100 150 200 250 300 350 400 450 500 Abundance #59136: Hexatriacontane AAAAA AAAA AAMAAAA A 4 I i 57 34.20 34.40 34.60 34.80 35.00 m/z 55.10 26.32% 5000 85 wwA M ’ ■ i , | Ll41... 239...... 379 407,435 , 478 506, miz-> 50 100 150 200 250 300 350 400 450 500 34.20 34.40 34.60 34.80 35.00

26006A.D NP112701.M Thu Dec 20 10:39:57 2001 Page 7

NYC-WTC_000030850

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