GCMS analysis results, sample AE09398, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAY1002\9398.D Vial: 6 Acq On : 10 May 2002 5:56 pm Operator: Sample : GC/MS SCAN 5/9 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Dotriacontanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.15 1.79 ug/1 129726 Chrysene-dl2 33.62

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 1-Dotriacontanol 467 C32H660 006624-79-9 70 2 3-Eicosene, (E) - 280 C20H40 074685-33-9 70 3 1-Docosene 308 C22H44 001599-67-3 70 4 17-Pentatriacontene______________ 491 C35H70 006971-40-0 70 Abundance Scan 2849 (31.147 min): 9398.D (-) m/z 55.10 100.00% 55

/ ^83 ................................................ 5000

111 30,80 31.00 31.20 31,40 1,4139 m/z 43.15 59.78% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #57795: 1-Dotriacontanol 57

83 5000 30,80 31,00 31.20 31.40 111 m/z 57.10 50.65%

I 1138, 196 200 250 300 350 400 420 448 450 mlz-> 50 100 150 Abundance #39521:3-Eicosene, (E)- 57 83 30,80 31,00 31.20 31.40 5000 m/z 73.10 41.56% 111

I J 1139 . 252 280 T—r-[—i—r—f—>—[—r m/z-> 50 100 150 200 250 300 350 400 450 Abundance #72943:1-Docosene 55 30,80 31.00 31.20 31.40 m/z 41.05 41.22% 97 5000

125

m/z—> 50 'I I , I ' 100 150 200 250 308......................................... 300 350 400 450 30.80 31.00 31.20 31.40 ■ ■ i ' ■ ■ ' i '

9398.D GCMS0510.M Mon May 13 09:12:48 2002 Page 2

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