GCMS analysis report for sample AE09524, May 2002

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Data File C:\HPCHEM\l\DATA\MAY0202\9524.D Vial: 22 Acq On 3 May 2002 11:38 am Operator: Sample GC/MS SCAN 4/22 FB Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 17-Pentatriacontene Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 31.17 6.30 ug/1 284647 Chrysene-dl2 33.64 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 17-Pentatriacontene 491 C35H70 006971-40-0 76 2 Phosphonic acid, dioctadecyl ester 587 C36H7503P 019047-85-9 76 3 5-Eicosene, (E) - 280 C20H40 074685-30-6 68 4 :1-Tetracosanol —---- ----------- /-------------- 354 C24H50O 000506-51-4 64 Abundance Scan 2851 (31.166 min): 9524. D (-) m/ z 55.10 100.00% 55

5000 83

113 1 l~ r l ' ' 1 1 l 1 30.80 31.00 31.20 31.40 31.60 ■ 1 r L 1,141 169 207 | r 1 । | rn i-_i J-1 r n | i i I i i i i i | I I । । । I i । । । r m/z 43.15 58.59% m/z—> 50 100 150 200 250 300 350 400 450 Abundance #58705: 17-Pentatriacontene 43

5000 83 T 1 T 1 o f MrY I I CPTMRTTP 30.80 31.00 31.20 31.40 31.60 , 111 m/z 57.10 49.84% I, . 11?9 . , . . . ...........................................462 490 ’ 1 r m/z-> 50 100 150 200 250 300 350 400 450 Abundance #60683: Phosphonic acid, dioctadecyl ester 55 83 MM 1 111 । 1) । i i m । i" 1 ।—।—। i 30.80 31.00 31.20 31.40 31.60 5000 m/z 73.10 41.69% 111

m/z-> ’ 'l 50 1 Illi 136 ! l r 111 I ' 100 150 ' 1

200 | ■

250 '

300 1

350 ' | 1 ' • 1 | 1 1 ' ' | 1 । ■

400 1 | ' r 1 1

450 | ‘ TT

Abundance #39520: 5-Eicosene, (E)- I | ! I 1l [ I I 1 | Pn I I | I |—I—|—|—I- 55 30.80 31.00 31.20 31.40 31.60 m/ z 41.10 40.49% 83 5000-

111

1 1 r , 1139 , 1 1 1 1 1 ' i 1 । ’ 252 280 | । । I i l । । i [ । i--? i [ । । । i । r ‘I Tin m/z-> 50 100 150 200 250 300 350 400 450 30.80 31.00 31.20 31.40 31.60

9524.D GCMS0501.M Fri May 03 12:28:34 2002 Page 2

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