GCMS analysis comments for sample AD28598, Dec 2001

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Data File : C:\HPCHEM\1\DATA\NOV3001\28651.D vial: 49 Acq On : 30 NOV 2001 2:41 pm Operator: 209 GALOS Sample : 11/23 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Phosphonic acid, dioctadecyl e Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 30.63 5.91 ug/1 1212130 Chrysene-dl2 33.03 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phosphonic acid, dioctadecyl ester 587 C36H75O3P 019047-85-9(81 2 5-Eicosene, (E)- 280 C20H40 074685-30-6 74 3 1-Heptadecene 238 C17H34 006765-39-5 72 4 1-Octadecene 252 C18H36 000112-88-9 55 Abundance Scan 2787 (30.627 min): 28651 .D (-) m/z 55.00 100.00% 55

43 83 5000 69 97 / — J 113127

mlz-> Trr 40 1lal4 60 80 141 153 169 183 197 211 225 239 253 267 295 . TTT . n ( TT . . I . . . . | . I . . ( I i I . I h . i . I r I I T I I । 11 I I 100 120 140 160 180 200 220 240 260 280 300 30.20 30.40 '30.60 30.80 31.00 m/z 43.05 52.00% Abundance #60683: Phosphonic acid, dioctadecyl ester 43- 5 5 69 83 97

5000 T I ' 1 ' ' I 30.20 30.40 30.60 30.80 31.00 111 136 m/z 57.00 49.56%

mlz-> we 40 60 - 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #39520:5-Eicosene, (E)- 55 J i • ■ ■ ' iT T T 83 30 20 30,40 30,60 30.80 31.00 5000 97 m/z 83.05 47.99% 70

miz-> Abundance 40 60 80 LE 111 139 252 1 ’11110017001—00110—— 280 100 120 140 160 180 200 220 240 260 280 300 #31657:1-Heptadecene 55 30.20 30'40 30.60 30.80 31.00 83 m/z 73.00 44.27% 97 5000 70 42 111

m/z--> TTTIr 1 1 40 60 1 . ...... . ' 1 1 ■■ T| * . 1 80 । ।। |b . । । । i i n । ri i । । ■ i i i । i 100 120 140 160 180 200 220 240 260 280 300 30.20 30.40 30.60 30.80 31.00 -PPP — r11' । r1 ।1

28651.D GCMS1126.M Fri NOV 30 16:42:58 2001 Page 4

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