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GC/MS analysis results for sample AD23322, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23322 conducted on October 15, 2001.

NYC-WTC_000088263–000088289

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088277
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C;\HPCHEM\1\DATA\OCT1201\23322.D Vial: 15 Acq On : 12 Oct 2001 3:48 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Phosphonic acid, dioctadecyl e Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T. 29.75 0.89 ug/1 92453 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phosphonic acid, dioctadecyl ester 587 C36H75O3P 019047-85-9 93 2 1-Nonadecanol 284 C19H40O 001454-84-8 93 3 Acetic acid, octadecyl ester 312 C20H40O2 000822-23-1 91 4 1-Nonadecene 266 C19H38 018435-45-5 81 Abundance Scan 2692 (29.751 min): 23322.D (-) rn/^ 43.05 100.00% 43

83 55 69 97 5000 111

■nfe-> Abundance juiyu 40 60 80 100 xx 125

120 139 153 ' 'I' ‘' I'' '' I'''' I' 140 160 180 #60683: Phosphonic acid, dioctadecyl ester 200 224 ' I ' ' ' ' I ' 220 240 29.40 29.60 29.80 30.00 m/z 83705 62.00%

55 69 83 43 97

' ‘ ' I ' ' ' ' I V 29.40 29.60 29.80 30.00 111 136 m/z 55.00 54711% 125 I ,Ji-,-II . .............................. . ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 ^kbundance #40236:1-Nonadecanol 55 69 83 97 V 29.40 29.60 29.80 30.00 5000 m/z 69.00 54.09%

u 111 31 42 125

il ' ' ' I ' ' “y-r-iXryjn-rT-p-rT-rqp-r-T-ryT-r-rT-p-rT-ryT-TT-rpr^^ 238 ■n/z-> Abundance 40

43 60 80 100 120 140 160 180 #73048: Acetic acid, octadecyl ester 200 220 240 , J.Uy.A,..... . 29.40 29.60 29.80 30.00 m/z 61705 52.80%

5000 83 97 61

V TlZz-> 40 60 80 100 120 140 160 180 200 220 240 29.40 29.60 29.80 30.00

23322.D NP091101.M Mon Oct 15 10:26:03 2001 Page 8

NYC-WTC_000088277

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NYC-WTC_000088277Source: NYC Law Department, mirrored locally

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