GCMS sample AE07115 results, April 25, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR2 202\7115.D Vial: 21 Acq On : 23 Apr 2002 4:39 am Operator: Sample : re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Phosphonic acid, dioctadecyl e Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.17 0.32 ug/1 44712 Chrysene-dl2 33.64

Hit# of 5 Tentative ID MW MolForm CAS# Qual 2 1 Phosphonic acid, dioctadecyl ester 587 C36H75O3P 019047-85-9(93 2 1-Eicosanol 298 C20H42O 000629-96-9 76 3 l-Docosene 308 C22H44 001599-67-3 68 4 4-Tetradecanol 214 C14H30O 001653-33-4 68 Abundance Scan 2845 (31.165 min): 7115.D (-) m/z 55.00 100.00% 55 __

5000 69 83 4' 97 /V 111 127 3080 31.00 31.20 31.40 ill • ■ i' • ! . Il. /I ■ ■ th . A , I I, , 141 m/z 43.05 53.98% mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #60683: Phosphonic acid, dioctadecyl ester 55 69 83 97

5000 Mr MwNy 30.80 31.00 31.20 31.40 111 m/z 57.00 51.71% 42 136 • ■ 1 * Tr TTT 1114 }’’111’1111 • i ■1 1 ■ I' ■ ■' i' ■ • ■ i • ■ ' ■ i ■ ■ mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72723:1-Eicosanol 43 $7 .A AA.A 83 97 30 80 31.00 31.20 31.40 5000 m/z 82.95 46.53% 70 111 125 * 1 1T It "I 1139 252 i■'■■I‘'‘I•■■■।1‘‘111 • ■i•■ ‘ • i ■ ■ ‘' i ■ ■ ■ ■ i ■ ■ • ■ i ‘'1 ■ i1 • miz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72943:1-Docosene 1 i 1 1 A 1 ■ ■ i • ‘ ■ ■ i ■ 55 30.80 31.00 31.20 31.40 m/z 69.00 43.14% 83 97 5000 70 111 42 125 ■11'1 i111 ‘ I .1139 ■ ■1 ■ । ■ ■ • • । ■ ■ ■ ■ । ' i ■ ■ ■ ■ i1 ■ ■ ■ i ■ ■' ■ i • ■ ■11 ‘ ‘ ■ i ■ ■ ' 308 ' I' ‘1 r AAA m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 30.80 31.00 31.20 31.40

7115.D GCMS0412.M Tue Apr 23 14:23:06 2002 Page 3

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