GCMS reference report, DEP Box 15, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY2902\12163.D Vial: 6 Acq On : 29 May 2002 4:15 pm Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Phosphonic acid, dioctadecyl e Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.02 1.19 ug/1 93759 Chrysene-dl2 33.47 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phosphonic acid, dioctadecyl ester 587 C36H75O3P 019047-85-9 76 2 1-Dotriacontanol 467 C32H660 006624-79-9 70 3 5-Eicosene, (E) - 280 C20H40 074685-30-6 68 4 3-Eicosene, (E) - 280 C20H40 074685-33-9 53 Abundance Scan 2830 (31.023 min): 12163.D (-) m/z 55.00 100.00% 55

83 5000

111 MIRTMT ■ • i ■ 1

, 1.1,1 30.60 30.80 31.00 31,20 31.40 m/z 57.00 55.04% mlz-> 5b 100 150 200 250 300 350 400 450 Abundance #60683: Phosphonic acid, dioctadecyl ester 55 83

5000 —AAA4AAAWA,AYMYNAY 111 30.60 30.80 31.00 31.20 31.40 136 m/z 83.05 53.37%

mlz-> ■ • i 50 1 — 100 1 150 1111++I+’’II 200 250 300 350 1 ■ 400 i ■ ■ 450 Abundance #57795:1-Dotriacontanol 57

83 ■ 0 30.60 30.80 31.00 31,20 31.40 5000 m/z 72.85 49.28% 111

- i 1,1139 9 1 ■ i ■ 420 448 ■ miz-s 50 100 150 200 250 300 350 400 450 Abundance #39520: 5-Eicosene, (E)- AA.A 1111 A,/ AA MAM. 55 30.60 30.80 31.00 31.20 31.40 m/z 69.05 48.14% 83 5000-

111

1 • । 1 ' i 1111?9................ 252 280 ............................. --40404 ' 1 ■ ' i ■ • 1 ■ i • ■ ■ 1 i 1 ■ 1 ‘ i 1 1 • • i ■ 1 1 ■ i 1 1 1 ' । 1 m/z—> 50 100 150 200 250 300 350 400 450 30.60 30.80 31.00 31.20 31.40

12163.D GCMS0528.M Thu May 30 08:42:05 2002 Page 3

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