GCMS reference report, DEP Box 15, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2902\12163.D Vial: 6 Acq On : 29 May 2002 4:15 pm Operator: Morgan Sample : gc/ms scan 5/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0528.M (RTE Integrator) *** Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Fluorononane Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 8.11 1.46 ug/1 120844 1,4-Dichlorobenzene-d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Fluorononane 146 C9H19F 000463-18-3 10 2 1H-Azonine, octahydro- 127 C8H17N 005661-71-2 7 3 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 7 4 2-Acetyl-1,4,5,6-tetrahydropyridine 125 C7H11NO 000000-00-0 3 Abundance ( Scan 334 (8.109 min): 12163.D () m/z 42.95 100.00%| <43

5000

125 ■ ■ ‘ i ■ ■ ■ ■ i ■ ■ ■ • i^i 1 i ■ 1 ■ ■ i 97

mz-> —I—————— 20 30 371 40 +FP-fLee— JL 50 60 70 80 90 100 110 117 II 1 120 130 7.80 m/z 124.90 8.00

1 8.20 8.40 20.71% |

Abundance #8922:1-Fluorononane 43

. .M 1 1 । 1 j * * । * 1 5000 56 7.80 8.00 8.20 8.40 27 70 84 . 97 m/z 96.90 13.70% 33 I - • > i > ■ 1 i ■ 1 miz-s 20 30 40 50 60 70 80 30 100 110 120 130 Abundance #4790: 1H-Azonine, octahydro- 30 56

70 ' 7.80 8.00 8.20 8.40 m/z 5000 81.80 10.50? 42 127 84 98

iz-> 20 ■ i ■ ■ 30 40 ■ • ।* 50 60 70 id v 80 90 ii2.120 .L I100. 110 130 . Abundance #4732: N-Acetylpyrrolidone - 43 7.80 8.00 8.20 8.40 | m/z 83.85 9.16%

5000

56 86 99 127 WMa/Woown 30 I -------- * I ‘ 69 * I ‘ ‘ 1 ■ I ’ ■ i ■ ■ ■ ,1 i ‘ 1 ■ ■ i112 ’ ■ ■ ■ i ■ ■ ■ 1 i ■ ■ 1 m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 7.80 8.00 8.20 8.40

12163.D GCMS0528.M Thu May 30 08:42:04 2002 Page 2

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