GCMS analysis report sample AE12098, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY3102\12098.D Vial: 6 Acq On : 31 May 2002 4:53 pm Operator: Morgan Sample : gc/ms scan 5/29 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.07 0.61 ug/1 39525 1,4-Dichlorobenzene-d4 12.06

Hit# of 5 Tentative- ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 40 2 Acetone 58 C3H60 000067-64-1 9 3 Acetic acid, 1,1-dimethylethyl este 116 C6H1202 000540-88-5 9 4 2 - Helpt anone, 7,7-dichloro- 182 C7H12C12O 000000-00-0 9 Abundance/ Scan 330 (8.071 min): 12098.D (-) m/z; 43.00 100.00% 43 /

59 5000

101 -PPP 7.808.00 8.20 8.40 51 —4 * '-'T' i‘ I - ■ ■ ■ I ■ ■ - ■ I 83 ■ ■ i ■ ■ ■ 1 i ■ ■ ‘ ■ i m/z 59.00 51.49% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 -------- 59 7.80 8.00 8.20 8.40 m/z 100.95 20.97% 15 31 _ 101 m/z-> | ■• i ■■ ■ ■ i • ■ ■ ■ i' • 10 20 I 30 TTT 1 ' ' l ' ''' 40 50 60 II,......... 70 83 80 .......... 90 1....110, 100 Abundance #62322: Acetone 43 7.80 8.00 8.20 8.40 5000 m/z 58.00 18.04% 58

... w... 27 +r, ^,,,.11,., '■'I11 I 1 ' ‘ • i ■ ■ ■ 1 i • ■ ■ ■ i ■ ■ ’ ‘ i • • • ■ i miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3292: Acetic acid, 1,1-dimethylethyl ester 43 7.80 8.00 8.20 8.40 m/z 41.00 8.51%

5000 57 101 15 27 • ' i ■ ■ ■ ■ i 1 ■ ■ ■ i ■ - • ■ i' 1 ' ' i 1 ■ T-h-rnr-r-r-pr-r-r-r-|-r-r-r-r-[-r-r-r-7-j-^^ n/z—> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

12098.D GCMS0531.M Mon Jun 03 09:34:20 2002 Page 1

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