GCMS analysis report sample AE12098, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY3102\12098.D Vial: 6 Acq On : 31 May 2002 4:53 pm Operator: Morgan Sample : gc/ms scan 5/29 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) . Title : 20*9 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.11 0.84 ug/1 54476 1,4-Dichlorobenzene-d4 12.06 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 40 2 2-Acetylthiazole 127 C5H5NOS 024295-03-2 4 3 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 4 4 2-Buten-1-amine, N-butyl-, (E) - 127 C8H17N 062337-86-4 4 Abundance Scan 334 (8.108 min): 12098.D (-) m/z 42.9.5 100.00%

L 43

5000

11' ■ ■ ‘~r TOIIT/TTE2d0/n1 97 125 7.80 8.00 8.20 8.40 37 49 *4 63 85 ii .119 |, m/z 124.90 11.84% “ I ■ ■ " I “ ■ ■ 1 *t 11 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247:2-Propanone, 1,1,1-trichloro- 43

5000 -------------------- 7.80 8.00 8.20 8.40 m/z 96.90 7.32% 15 35 ,49 85 97 117 125 ■ ' i ■ ' ■ ■ i ■ ■ ■ ■ i ■ 1 I' 1 ' ''l • 11 ■ 11 > '■ < j < ■ ■ ■ 11— 11 ■ ■ ■ 'I ■ • ■ ■ i ■ ■ *4l • • * * I ■ ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4717:2-Acetylthiazole 43 “* ‘ ‘ I * * .' • I ‘ ‘ ‘ I ‘ 1 1 1 I 1 ‘ 1 1 ! 7.80 8.00 8.20 8.40 5000 m/z 126.85 6.89% 99 127 58 112 85 33 ------PPP ■ ■ i • ■ ‘ ■ i • ■ ■ ■ i ■ 1 ■' i • * • ■ i • • 1 ■ i ■ ■ ■ ri ■ ■ • miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4732: N-Acetylpyrrolidone 1 ■ ■ i ' ■ ' ■ i ■ ■ ■ ■ i ■ ' 1 ■ i 1 ■ ■ ■ 1 43 7.80 8.00 8.20 8.40 m/z 84.95 6.48%

5000 99 127 56 M 86

n/z-> ■ ■ i ■ ■ ■ • i ■ ■ 10 20 30 40 19 50 60 70 80 —. 1... 112.... pos 90 100 110 120 130 1 ■ i ■ ■ ■ ■ i ■ ■ ■ ■ । ■ ■'111 11' i 7.80 8.00 8.20 8.40

12098.D GCMS0531.M Mon Jun 03 09:34:21 2002 Page 2

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