GCMS analysis report sample AE12094, June 2002

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GCMS laboratory analysis report for sample AE12094 showing unknown compounds and surrogate recovery data from June 6, 2002.

NYC-WTC_000014976–000014986

Folder label: “GCMS X 5/30/02 A 6/1/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\MAY3102\12094.D Vial: 17 Acq On 1 Jun 2002 3:44 am Operator: Morgan Sample re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C>\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) ** Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone,•1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 8.11 0.85 ug/1 58758 1,4-Dichlorobenzene-d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 36 2 1-Fluorononane 146 C9H19F 000463-18-3 9 3 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 9 4 2-Acecylthiazole 127 C5H5NOS 024295-03-2 5 Abundance k Scan 334 (8.108 min): 12094.D (-) m/z 42.90 100.00% 43

5000

125 EETrnmdts , ! , 1110221" 49 == 63 97 83 7.80 8.00 8.20 8.40 -n-p 37 • i ' ■ ‘ ■ i ■ ' I'1 i ' Apadvosgossartha II i • * • ‘ i ' • ■ ■ i ■ ■ ■ ■ i ■ • ■ ■ i • ■ 119 m/z 124.90 15.06% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247:2-Propanone, 1,1,1-trichloro- 43

5000 ‘ * 1 i ■ ■ 1 ' i ■ ■ i ■ ■ 1 ' l ■ ■ ■■■ I 7.80 8.00 8.20 8.40 m/z 96.90 10.86% 15 ■ ■ i ■ ‘ l ■ ■ • • i' 35 11 ,49 ■ l'i ‘ ‘1 i * ‘ 11 i • ■ 1 ‘ i1 85 97 117 125 -+111,11,111,7/11/1,1,/1/212/1/1)/2, miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #8922:1-Fluorononane 43 ' 1 i ' 1 ■ • i ■ ■ ■ i ■ ‘ ‘ ■ i ■ ■ ■ ‘i 7.80 8.00 8.20 8.40 5000 m/z 126.85 9.53% 56 27 70 84 97 33 I ■ | 1 ■ ■ i • • ' I' • ■ • i1 • ■ i ‘ ‘ ■11' ■ • ■ । ■ i ■ • ■111 • m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4732: N-Acetylpyrrolidone ‘ ‘ ■ i ‘ ■ ■' 1 I ‘ 1 1 1 I ' 1 1 1 1 1 1 ' 1 1 43 7.80 8.00 8.20 8.40 m/z 82.95 9.15% 5000 99 127

m/z—> 30 ■ ■ i ■ ■ ■ ‘ i ‘1 1 111 '' 11 10 20 30 40 56 69 1 ‘ i1 •1 ‘ i 11 ■ • i111 * i' 50 60 70 80 86 , 112 ■ t • ■ • 11 * ■ ‘ ■ i ’ • ■ ■ i ■ • ■ 1 i ■ ■

90 100 110 120 130 ..... .14..... . ‘ ' I ‘ ‘ 7.80 ' I ‘ ‘ ‘ ' I ‘ 8.00 8.20 ‘ ‘ I ‘ ‘ 1 1 I 8.40

12094.D GCMS0531.M Mon Jun 03 11:44:32 2002 Page 2

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