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GCMS analysis report sample AE12094, June 2002

Machine-extracted title · confidence 95%

GCMS laboratory analysis report for sample AE12094 showing unknown compounds and surrogate recovery data from June 6, 2002.

NYC-WTC_000014976–000014986

Folder label: “GCMS X 5/30/02 A 6/1/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\MAY3102\12094.D Vial: 17 Acq On 1 Jun 2002 3:44 am Operator: Morgan Sample re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : CAHPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) ** Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 25.56 0.41 ug/l 39789 Phenanthrene-dl0 25.42

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene -d10- /4 188 C14D10 001719-06-8(87 2 Phenanthrene -d1 07 188 C14D10 001517-22-2 40 3 Pentacyclo[/.4.0.0(3,7) .0(4,14) .0(6 188 C14H20 000000-00-0 36 45(4H)-Isoxazolone,4,4‘-bis[3-methy376C22H20N204 000000-00-0 28 Abundance Scan 2235 (25.560 min): 12094.D (-) m/z 188.10 100.00% 118

5000

80 94 160 A 25.20 25.40 25.60 25.80

miz-> 42 52 66 1" 11'1' 11 “ 11111' 111'1 tTTITTTTTTTTTTT —ll m/z 94.00 18.80% 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

5000 25.20 25.40 25.60 25.80 m/z 189.10 17.35% 66 80 । 94। 160 । ITT 11 >>> 1111111111J i ■ " 111" I' ‘' I' “ ‘ 1 ‘" I' " ‘ I ■ — miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

25.20 25.40 25.60 25,80 ' ‘' 5000 m/z 184.10 14.80%

80 94 160 66 mz-> Tp-rrrp- 40 50 i1 ■ • ■ r 111 ■ ■ l ■1 ■ ■ |1'111 " 1' I' " H 1 " 1!1'1 0 “ 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ..... Il.. Abundance #19959: Pentacyclo[8.4.0.0(3,7).0(4,14).0(6,11) tetradecane 1*11111**1* 188 25.20 25.40 25.60 25.80 m/z 80.00 13.61% 5000 79 92 117 145 159 173 106 131 —mmmmmmpm ‘I -H "i “ “ i Tu ‘111 ....... 1,...... 1...... I . 1111111 ‘ ‘1111111 “ TT TKnnmagmTgT iz—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 2520 25.40 25.60 25.80

12094.D GCMS0531.M Mon Jun 03 11:44:33 2002 Page 3

NYC-WTC_000014985

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NYC-WTC_000014985Source: NYC Law Department, mirrored locally

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