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← Document results/DEP Box 28/GCMS X 1/3/02 A 1/24/02
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GCMS analysis results for sample AE00007, Feb 13 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE00007 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050165–000050176

Folder label: “GCMS X 1/3/02 A 1/24/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2402\7.D Vial: 6 Acq On : 24 Jan 2002 5:57 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Anthracene-dlO- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

24.90 0.23 ug/1 85334 Phenanthrene-dl 0 24.76

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene 2 Phenanthre 10-32— -did 188 C14D10 188 C14D10 001719-06-8 001517-22-2 72 64 3 5(4H) -Isoxazolone, 4,41-bis[3-methy 376 C22H20N2O4 000000-00-0 37 4 Pentacyc . 4.0.0 (3,7) . 0 (4,14) .0(6 188 C14H20 000000-00-0 33 Abundance Scan 2163 (24.905 min): 7.D (-) m/z 188.10 100.00% I 188 I

i 5000-

94 ‘ I‘ 1 I ’ ’ ' 1 I '■'■■'■■’"I 13 158 24.60 24.80 25.00 25.20

miz-> 42 66 I j TId—trtr ,137.1.. . F • ■ ■ i ■1 ■' r • ■' r ■ ■ ‘ i • ■ ■ ■ i ■ • ■ • I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 I-' I m/z 9 . 95 20.32% Abundance #19957: Anthracene-d 10- 188

5000 24.60 24.80 25.00 25.20 m/z 189.10 20.31% 66 , 94 160 , ■ii_____ t I '11' I'' H I Tn I ’' ‘ I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance I #19958. Phenanthrene-d10 188 01141 — 24.60 24.80 25.00 25.20 5000- m/z 184.05 16.30%

80 160 ! I • I' ‘’ I' • "I" '' I '' i " ■' i'' " I'' " r ' " i " " I I’TTT I ’' " I1 • ’11 " '' I'' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #51906: 5(4H)-Isoxazolone. 4,4'-bis[3-methyl-4-(phenylmethy ......./ y......................... 188 24,60 24.80 25.00 25.20 m/ z 80.05 10.72% 91 5000-

115 . — 215 241 I n 144nuTT 170 332 376 / ‘IT I ■ * ■' I Tmm i " ■ ■ i ■ " ■ i ■' ■ ■ i ‘' ■ i' ■ " r " ' i ’11 ’ I m-p T i ■ ■ ■ > । ■ i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 24.60 24.80 25.00 25.20

7.D GCMS0208.M Fri Feb 08 13:41:27 2002 Page 4

NYC-WTC_000050175

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NYC-WTC_000050175Source: NYC Law Department, mirrored locally

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