GCMS calibration table data, DEP Labs, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY3002\11284.D Vial: 11 Acq On : 30 May 2002 11:55 pm Operator: Morgan Sample : re-ext Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) .4 Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Anthracene -d10- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 25.57 0.41 ug/1 46324 Phenanthrene-dl0 25.43 . Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 80 2 Phenanthrene -diO 188 C14D10 001517-22-2 47 3 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 36 4 Cyclohexanone, phenylhydrazone 188 C12H16N2 _______000946-82-7 36 Abundance Scan 2236 (25.569 min): 11284.D (-) " m/z 188.10 100.00% 1)18

5000

94 25.20 25.40 25.60 25.80 ■ 42.55 66 80 -# 11 > i ■ ■ i " । ■ i “111 ■ m/z 189.10 15.31% mht~> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 118

5000 ‘ I TT 25.20 25.40 25.60 25.80 m/z 94.00 11.91% 66 80 94 160 q T > । 11 n । i 11 । । i rr i । i i i i । ti i i ] i i i i । । । 11 | i i i 11 i i i i । |•l'|l I’T mZz—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 118

25.20 25.40 25.60 25.80 5000 m/z 184.10 11.70%

80 160 66 ... I E i■■■■ i ■ ■ ■ ■ i " ■ ■ i ■■■■i "'' I'1 n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19913: Naphthalene, 1,7-dimethoxy- 173 108 25.20 25.40 25.60 25.80 ‘ ‘ m/z 187.20 11.37%

5000 102 115 145

51 63 75 94 130 158 • ■ । “1' f' “ ■ i “ i "’> ■ i ■' “ i ■ । " i TTIPgT | 1 ‘ i “1' I “ ‘' i •"' i1 ITT ‘T "di8 n/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.20 25.40 25.60 25.80

11284.D GCMS0520.M Fri May 31 11:33:59 2002 Page 2

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