GCMS unknowns report, DEP Box 15, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAY2902\12170.D Vial: 12 Acq On : 29 May 2002 10:09 pm Operator: Morgan Sanpl e : gc/ms scan 5/23 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P g*t

Quant Method : C:\HPCHEM\1\METHODS\GCMS0528 .M (RTE Integrator) += Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

25.57 0.43 ug/1 47014 Phenanthrene-dl0 25.43

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-d10- 7 7 188 C14D10 001719-06-8 90 2 Phenanthrene-d10 188 C14D10 001517-22-2 (78 3 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 42 4 4H-Pyrido[1,2-a]pyrimidin-4-one, 3- 188 C11H12N2O 057773-19-0 40 Abundance Scan 2235 (25.566 min): 12170.D (-) m/z 188.10 100.00% 118

5000

80 94 1 ‘i1' • ■ i ■ 66 160 25.20 25.40 25.60 25.80 • ■ i ■ ''i ■ -H 49 — m/z 94.00 16.72% 111 i ■ ■ ■ ■ i • ■ ■ ■ i ■ •1' i ‘ ■11 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d1 0- 188

5000 25.20 25.40 co 25.80 m/z 80.00 16.36% 160

niz-> q 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 11® • i • • " 1 i * ■ i 1 25.20 25.40 25.60 25.80 5000 m/z 189.10 13.94%

«> 94 160

miz—> L 120 130 140 150 160 ....... .................... 66 40 50 60 70 80 90 100 110mgm I*... 170 180 190 Abundance #19913: Naphthalene, 1,7-dimethoxy- *I***111144a/nI1I 173 188 25.20 25.40 25.60 25.80 m/z 184.10 13.35%

5000 102 115 145

51 83 " i ■ " ■ i ' "111,1" I 75 11 TPPT 94 " i11 ■ ■ i ■ , 130 . 158 ' i " “ i ■ ■ ■' i " " i ■ I 188 I iz—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.20 25.40 25.60 25.80 '' 1'

12170.D GCMS0528.M Thu May 30 08:43:14 2002 Page 3

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