GCMS analysis report sample AE12094, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\MAY3102\12094.D Vial: 17 Acq On 1 Jun 2002 3:44 am Operator: Morgan Sample re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C?\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) *= Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.06 1.44 ug/1 99463 1,4-Diehlorobenzene-d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 59 2 Acetone 58 C3H60 000067-64-1 12 3 5-Hexen-2-one 98 C6H10O 000109-49-9 9 4 3 -Hydroxy-2-pentanone 102 C5H10O2 003142-66-3 9 Abundance Scan 329 (8.063 min): 12094.D (-) m/z 43.00 100.00% 43

59 5000

101 3051102T21T7 • • ' 1 i •’ 7.801 8.00 8.20 8.40 ■ ■ i ■ ■ ■ 1 I 1 1 1 ' I 1 ' 1 ’’1 +-53-1 1 1 1 ‘ 1 1 1 1 1 1 1 ‘ 83 1 1 1 ' 1 1 1 1 ‘ 1 ' 1 1 1 m/z !59.00 50.93% mz-> 10 20 30 40 50 60 70 80 90 1(X) 110 Abundance #64275:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 TT°|-| ■) 1 11 111/4/441 4 I ■ ■ 59 7.80 8.00 8.20 8.40 m/z 58.00 19.00% 15 31 . 101 | । ......... . .................... ............. ' ‘ i ■ ■ ■ ■ i ■ ■ ■ 1 I' ■ TT 1*14’1 miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62322: Acetone 43 7.80 8.00 8.20 8.40 5000 m/z 101.05 17.63% 58 27 — i ' ■ ' ' i ‘ ‘ ' ■ i ■ ‘ 1 ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ miz-> 10 20 30 40 50 60 70 60 90 100 110 Abundance #63205: 5-Hexen-2-one ___________ / AAA ’ * ' * I ‘ ‘ ‘ * I ‘ ‘ ‘ ' I 43 7.80> 8.00 8.20 8.40 m/z •40.95 7.61% 5000

27 55 15 50 . | I ‘ ■ i ■ ‘ 1 1 1 1 1 1 1 1 1 1 38,4 1 ' I ‘ ‘ ' T 14,4,’1411+14483 98 ■ ■ i ■ ■ • 1 1 1 ''1 1 1 1 1 mfz-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

12094.D GCMS0531.M Mon Jun 03 11:44:31 2002 Page 1

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