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GCMS analysis results for sample AE12677, June 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12677 conducted on June 6, 2002.

NYC-WTC_000015027–000015035

Folder label: “GCMS X 5/30/02 A 6/1/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\l\DATA\MAY3102\12677.D vial: 22 Acq On 1 Jun 2002 8:39 am Operator: Morgan Sample gc/ms scan 5/30 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.06 1.28 ug/1 84778 1,4-Dichlorobenzene-d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 42 2 5-Hexen-2-one 98 C6H10O 000109-49-9 9 3 Acetone 58 C3H60 000067-64-1 9 4 3-Hydroxy-2-pentanone 102 C5H10O2 003142-66-3 9 Abundance Scan 329 (8.064 min): 12677.D (-) m/z 43.00 100.00% 43 59 5000

101 mu/mn—moTTTRR 7.80 8.00 8.20 8.40

niz-s 10 20 30 -3L40 +53+ 50 60 83 -PP---C 1 r I i ' 1 1 r i 1 70 80 90 100 110 m/z 59.0.0 51.53% Abundance #64275:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.80 8.00 8.20 8.40 m/z 58.0.0 20.00% 15 31 — 101 I I 83 । TTT 11" i • ■ ■ ■ i 1 1 1 1 i ■ '■ ■ 1 i ' 1 1 1 1 1 1 1 ' i 1 miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63205:5-Hexen-2-one 43 1 I ' 1 1 1 1 1 1 '1 f 1 1 ' 1 1 1 7.80 8.00 8.20 8.40 5000 m/z 101.05 19.08%

27 55 15 50 . | ........ r........ 1........ 38, 83 98 ■ ‘ I ‘ ‘ ‘ I ' ‘ ' I ‘ ‘ I ' ' 1 I ■ ■ ' 1 1' miz—> 10 2030405060 70 8090 100 110 Abundance #62322: Acetone 1 1 i ■ ■ 1*’’I 43 7.80> 8.00 8.20 8.40 m/z •41.00 8.49% .......................... 5000 58 27 11* + 1 ’ *444/421" I • ‘ ' I 1 ' 1 1 T‘ ' I ‘ ‘ 1 1 1 1 1 ' ' 1 1 1 ' I 1 1 m/z—> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

12677.D GCMS0531.M Mon Jun 03 11:45:50 2002 Page 1

NYC-WTC_000015034

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NYC-WTC_000015034Source: NYC Law Department, mirrored locally

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