GCMS calibration data AE12095, DEP Labs, May 2002

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY3002\12096.D vial: 15 Acq On : 31 May 2002 3:50 am Operator: Morgan Sample : re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P 2*.* Quant Method : C:\HPCHEM\1\METHODS\GCMS0520 .M (RTE Integrator) -= Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.07 0.93 ug/1 71002 1,4-Dichlorobenzene-d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl - 116 C6H12O2 000123-42-2 59 2 5-Hexen-2-one 98 C6H10O 000109-49-9 9 3 Acettone 58 C3H60 000067-64-1 7 4 2-Propanone, 1-cyclopropyl-______ 98 C6H10O 004160-75-2 5 Abundance Scan 329 (8.068 min): 12096.D (-) m/z 42.90 100.00% 43

5000 59

51 83 101 7.80 8.00 8.20 840’1 mRRH m/z 59.00 47.82% miz—> 5 10 15 20253035404550556065 70 75 80859095 100105 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.80i 8.00 8.20 8.40 m/z 58.001 19.46% 27 ।>. <.,...111... ।. 1111li । ij n 111il +49+ 83 101 J.... |.... ।.... ।... . ।.. I. ।. ... ।.... (.. 1., I ni 1111111 miz—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63205:5-Hexen-2-one 43 1 i • » 7.80 8.00 8.20 8.40 5000 m/z 101.05 17.55%

27 55 15 2. I I 38,. 50 . 83 98 11111।111 [ ।, u 11 u 111I11 (TTIt 11 n 11II I1 u 111111i I, (i 11iii [ 111i1111 ipi 111111 rpi i11111111iI111,i111। n 11 /z—> 5 10 15 2025303540 45 50556065 70 75 80859095 100105 Abundance #62326: Acetone 40 7.80 8.00 8.20 8.40 m/z 41.00 8.34% 5000

27 36 58

—A— A-AAMAMA k m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 7.80 8.00 8.20 8.40

12096.D GCMS0520.M Fri May 31 11:34:55 2002 Page 1

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