GCMS analysis results sample AE12156, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY2402\12156.D Vial: 10 Acq On : 25 May 2002 12:25 am Operator: Morgan Sample : gc/ms scan 5/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:»\HPCHEM\1\METHODS\GCMS0520 .M (RTE Integrator) *5 Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.12 10.46 ug/1 793511 1,4-Dichlorobenzene-d4 12.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 78 2 Acetone 58 C3H60 000067-64-1 16 3 Propanenitrile, 3-ethoxy- 99 C5H9NO 002141-62-0 9 4 5-Hexen- 2 - one 98 C6H10O 000109-49-9 9 Abundance Scan 334 (8.115 min): 12156.D (-) m/z 42.95 100.00% 43

5000 59

101 11 ' । 1 ■ ■ ■ i • • ■ • i 1 ■ ■ 1 i ■ ■ ■ ■ i 7.80 8.00 8.20 8.40

m!z-> —34 I ‘'1 i 53 , 69 83 1mmmuHptr-rp-rrrp-n 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 m/z 59.00 44.42% Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 / 59 7.80 8.00 8.20 8.40 m/z 58.00 22.27% 27 . 101

miz—> mm +49 1-1mmmmmPImITmTP 83 | 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #62322: Acetone 43

7.80 8.00 8.20 8.40 5000 m/z 101.05 16.55% 58

*PWago 119911m3903r1—0190—1——2—BIUT—n m/z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #63285: Propanenitrile, 3-ethoxy- /......... ■ ■ i • ■ • ■ i ■ ■ j ‘ • i 31 7.80 8.00 8.20 8.40 m/z 41.00 6.36% 54 5000 59

26 45 • |I .. ,. !, 1, .1 !. I1 , I |।11| 1 .1 11. .. ,.. ,, ,. Ii ., f,. ., !,, ,. .. ,., i ,.. ., ! ., ,, t98 . 1,!., .. !,, ,, ! ,, , miz—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 7.80 8.00 8.20 8.40

12156.D GCMS0520.M Tue May 28 12:04:41 2002 Page 1

NYC-WTC_000013376