GCMS calibration data AE12095, DEP Labs, May 2002

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY3002\12096.D Vial: 15 Acq On : 31 May 2002 3:50 am Operator: Morgan Sample : re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P ?* Quant Method : C:\HPCHEM\1\METHODS\GCMS0520 .M (RTE Integrator) - Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Hexyl octyl ether Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 8.10 0.77 ug/1 58917 1,4-Dichlorobenzene-d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexyl octyl ether 214 C14H30O 000000-00-0 10 2 Pentacosane 352 C25H52 000629-99-2 9 3 Hexadecanol 242 C16H340 029354-98-1 9 4 Oct 2,7-dimethyl- 142 C10H22 001072-16-8 9 Abundance Scan 333 (8.105 min): 12096.D (-) m/z 42.90 100.00% 43

5000 125 —i -r r-|-ri i 1 i i i । ■ iTi-]TTTT | 63 85 97 7.80 8.00 8.20 8.40 V'. h40i . il ■ ■ i ■ Ini 1 i 1 ■ II ii ■ ■ i ' ■ ■ ■ i 1 ■ ■ ■ i 1 ■ ■ ■ i ■ ' ■ ■ i ■ ■ ■ ■ i ■ ‘ ■ ■ i • ■ m/z 124.85 22.31% miz-> 20 60 80 100 120 140 160 180 200 220 Abundance #26415: Hexyl octyl ether 43 57 85 71 5000 ■ ■ • i ■ ■ ■ • । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ ■ • ■ । 7.80 8.00 8.20 8.40 m/z 42 00 18.97% 112 i ■ ■ 1 ■ i ■ ■ . . Illi i 1 i ' 1 ■ ■ i 1 miz-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #73718: Pentacosane 40 57 ■i-r| rr-i i । i i i i ।

71 7.80 8.00 8.20 8.40 5000 m/ Z 126.85 16.91% 85

99 113 127 141 155 169 183 197 211 225 s 20 40 60 MU ' ‘ I ■ ' ■ ■ | • ■ • ■ | | > ' ■ ' | । T-r । i i i i । i ■ 80 100 120 140 160 180 200 220 Abundance #32431: Hexadecanol f 1 43 7.80 8.00 8.20 8.40 m/z 96.90 14.97%

5000 27 1 82 56 68 96 r , ■ II, 199 11 । । । ' > । । । । > । 1 n/z—> 20 40 60 80 100 120 140 160 180 200 220 7.80’ 8.00 > 8.20 8.40

12096.D GCMS0520.M Fri May 31 11:34:56 2002 Page 2

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