GCMS analysis results for sample AE12675, June 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12675 conducted on June 6, 2002.

NYC-WTC_000015016–000015026

Folder label: “GCMS X 5/30/02 A 6/1/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\MAY3102\12675.D Vial: 20 Acq On 1 Jun 2002 6:41 am Operator: Morgan Sample gc/ms scan 5/30 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P 2* Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) . Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 8.11 0.96 ug/1 65003 1,4-Dichlorobenzene-d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 9 2 1-Fluorononane 146 C9H19P 000463-18-3 9 3 4,5,6yfri-O-acetyl-2,3-di-O-methyl- 331 C14H21NO8 059061-07-3 4 4 2-Propanone, 1,1-dichloro- 126 C3H4C12O 000513-88-2 4 Abundance Scan 334 (8.113 min): 12675.D (-) m/z 43.00 100.00% 43

5000

125 rTo——TTDDTDTu’i 7.80 8.00 8.20 8.40 63 —... I1, . 1 .., n . .......... 1 85 97 . m/z 124.85 15.90% miz-> 20 40 60 80 100 120 140 160 180 ‘260' ‘226* 246' ‘260' ‘ ‘ ‘ Abundance #12247:2-Propanone, 1,1,1-trichloro- 43

5000 7.80 8.00 8.20 8.40 m/z 126.85 11.89% 15 ■ • i 1 1 1 ■' i 85 97 125 TT TTTTTTTTTTTT00] miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #8922:1-Fluorononane 43 ■ ' ■ i ■ ‘ ■ i • • ■ ■ i ■ ■ ■ 1 1 ■ 1 ' • 1 7.80 8.00 8.20 8.40 5000 m/z 96.90 9.85% 56 27 70 84 97

■ ■ 1 ■ ■ ■ ■ 1' ■ 1 .1 II 1 1 ■ ■ ■ • 1 ■ •i 1 * ■ ■ i ■11 ■ i ■ ■ ■ ■ i ■ • ■ ■ i ■ ■ ■ • i ■11 111' '111111111111 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #47003:4,5,6-Tri-O-acetyl-2,3-di-O-methyl-D-mannonitrile • ‘ । ■ 1 ■ • । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ • ■ • । 43 7.80 8.00 8.20 8.40 m/z 84.85 7.87% 5000

85 99 44=127 ■ ■!11 ■ • 1 • ■ ■ ■ 1 • 1141 "TT* 1 11“ “ I ’ * 1.1 11' 201 ■ '11' • ■ ।187 * ■ > f * 1" 159 ■ r ■ ■..... 1 ■ 1 *11261 ■..... 111 ■ t ■ 111111 1 1 i ■ ■ 1 ■ i ‘ 1 ■ ■ i • 1 • ■ i ■ ■ • • i m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 7.80 8.00 8.20 8.40

12675.D GCMS0531.M Mon Jun 03 11:45:22 2002 Page 2

NYC-WTC_000015024

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