GCMS analysis results for sample AE12570, June 2002

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Laboratory report documenting GCMS analysis of sample AE12570 conducted on June 7, 2002, including surrogate recovery data.

NYC-WTC_000014680–000014689

Folder label: “GCMS X 5/28/02 A 6/4/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\JUN0302\12570.D Vial: 21 Acq On 4 Jun 2002 4:56 am Operator: Sample gc/ms scan 5/28 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 8.11 0.86 ug/1 55130 1,4-Dichlorobenzene-d4 12.07 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 38 2 Heptacosane 380 C27H56 000593-49-7 9 3 Decane, 1-fluoro- 160 C10H21F 000334-56-5 9 4 1,3,5/Triazin-2(1H)-one, 4,6-diamin 127 C3H5N50 000645-92-1 9 7 Abundance Scan 334 (8.114 min): 12570.D (-) m/ z 43.00 100.00% 43

5000

125 **n,m———m—TrT2TT 61 97 7.80 8.00 8.20 8.40 TN 44 li Jal "th mmmmnpmmmpmmmmmmmT m/z 124.95 16.92% mtz~> 20 40 60 80 100120140160180 200220 240260 280300 320 340 360380 Abundance #12247:2-Propanone, 1,1,1-trichloro- 43

1 5000 7.80 8.00 8.20 8.40 m/ z 126.85 11.64% 15 85 125 . .111. V.. ।। f, 11"| h . .'I।rr 1111111111111,111, n । ■ 1111 ii h 1111 ""i' miz-> 20 40 60 80 100120140160180200220 240260 280300 320340360380 Abundance #74082: Heptacosane 43 ■ ■ ■ i ■ ■ ■ 1 i • • • ■ i ■ ■ ■ ■ i ■ ■ • ■ ।

71 7.80 8.00 8.20 8.40 5000 m/z 96.90 10.95%

99 1A127 183 211 253 353 380 “'' i “ “ i • ■' ।. 1* ’1’6+411—141191981—2880——8714 ITT"4 111 n iT| 11 11 |ttt i yr 1111 n n-p-rn । 144/1411 mlz-> 20 40 60 80 100120140160180 200220 240260 280300 320340 360 380 Abundance #12496: Decane, 1-fluoro- ■ ■ ■ i ■ 1 • ■ i ■ ' ■ ■ i ■ 43 7.80 8.00 8.20 8.40 rn/z 84.85 8.48%

5000 70 97 ...... , I TTrryrr+ryVrr 116................................ ................... 1 ■ i ■ ■ ■ 1 I ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i m/z-> 20 40 60 80 100120140160180 200 220 240 260 280300 320340 360380 7.80 8.00 8.20 8.40

12570.D GCMS0531.M Tue Jun 04 11:52:35 2002 Pace 2 NYC-WTC_000014688

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NYC-WTC_000014688Source: NYC Law Department, mirrored locally

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