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GCMS analysis results for sample AE12672, June 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12672 conducted on June 6, 2002.

NYC-WTC_000014943–000014952

Folder label: “GCMS X 5/29/02 A 5/31/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY3102\12672.D Vial: 12 Acq On : 31. May 2002 10:49 pm Operator: Morgan Sample : gc/ms scan 5/29 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 1 R.T. EstConc Area Relative'to ISTD R.T. 8.10 0.95 ug/1 62154 1,4-Dichlorobenzene-d4 12.06 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 33 2 1-Fluorononane 146 C9H19F 000463-18-3 9 3 Ethanol, 2,2,2-trichloro- 148 C2H3C130 000115-20-8 9 4 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 5 Abundance ' Scan 333 (8.105 min): 12672.D (-) m/ z 42.95 100.00% 43

5000

—mTTTTT 36 __ 63-TTP Tm 83 97 Ji 11711 127 II, 7.80 m/z 126.85 8.00 8.20 8.40 9.11% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #12247:2-Propanone, 1,1,1-trichloro- 43

5000 • * ■ । 1 ■ 1 ■ i ' • ■ ‘ I 1 1 1 1 1 1 1 1 1 I 7.80 8.00 8.20 8.40 m/z 124.95 9.04% 15 135, 1' '’1 ■ । ■ 1111111 ■ 85 Tpr I 1 ‘ 97 117 125 tt • ■ ‘ i | ■ n'l i UTlB . 11 p i ■ i । i । miz—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #8922:1-Fluorononane 43 1 • 1 1 ‘ Tnfn l i I I I IJ I I I I J j 7.80 8.00 8.20 8.40 5000 m/z 82.85 7.66% 56 27 70 8497 1 - tttt ----- ■ ■ i " ■ ■ t ■ ■ • ‘i ■ " ' i ‘ 4*4 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66531: Ethanol, 2,2,2-trichloro- 31 7.80 8.00 8.20 8.40 m/z 96.80 7.54% 5000 49 77

Il 61 ' ■ | “ 1 ‘ I ‘ 1 “1 1 ' “ I 1 1 '' I 1 1 1 ' ?• 1 1 •| 1 84 113 . 2,100000000001111.150/ * < i * • - > i * < . . । . i . i j . j mfz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 7.80 8.00 8.20 8.40

12672.D GCMS0531.M Mon Jun 03 09:35:44 2002 Page 2

NYC-WTC_000014951

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