GCMS analysis results for sample AE06457, April 2002

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1702\6457.D Vial: 15 Acq On : 17 Apr 2002 9:54 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 8.25 0.34 ug/1 41295 1,4-Dichlorobenzene-d4 12.21 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanohe, 1,1,1-trichloro- 160 C3H3C130> 000918-00-3 33 2 Ethanol, , 2,2-trichloro- 148 C2H3C130> 000115-20-8 4 3 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 4 4 1-Fluorononane 146 C9H19F 000463-18-3 4 Abundance Scan 349 (8.252 min): 6457.D (-) m/z 42.95 100.00% 43

5000

InOOn—n.m Tad I I | I v । 97 125 8.00 8.20 8.40 8.60 _____________ 36 , 151 6371 83 ' ' i 1 1 1 1 i 1 ' ' ' i 1 1 + ' ■ ■' i 1 ■' ■ i ‘। '1111'' i' 1II i1 ■111 ■1'11 1171 i ■''1 i m/z 124.95 11.89% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #12247:2-Propanone, 1,1,1-trichloro- 43

- 5000 ‘ i ■ ■ 1 1 i 1 ■ 1 3.00 8.20 8.40 8.60 I m/ z 46.95 7.78% 15 35 85 97 117 125 TTTOmPTTTT ' r ' ■' i < 11 1 ।1 । rc| 11l 1’1’11’1111—1 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66531: Ethanol, 2,2,2-trichloro- 31 lllf'i!JIM* m/z 8.00 8.20 96.95 8.40 8.60 7.65% I 5000 49 77 113 84 . 1. 61. + 150 "1 ‘ 11111111111111011IT7rT 1 ' I ' ' 11 1 1 '"I" "I1 I ‘ ‘‘ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #4732: N-Acetylpyrrolidone 43 8.00 8.20 8.40 8.60 m/z 82.75 6.47% 5000

99 127 86

m/z—> —PH 30

10 20 30 J 40 56 । TPPPTTTT 50 60 69 70 ML 80 90 112 I '1 1' i'' 1 1 1 100 110 120 130 140 150 i' 1111'' 8.00 8.20 ■ ■ । • ■ ■ ■ । 8.40 .60 ■

6457.D GCMS0412.M Thu Apr 18 09:15:29 2002 Page 2

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