GCMS analysis results for sample AE06457, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\1\DATA\APR1702\6457.D Vial: 15 Acq On : 17 Apr 2002 9:54 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 8.10 2.23 ug/1 269837 1,4-Dichlorobenzene-d4 12.21 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, ter:ramethyl- 88 C4H12Si 000075-76-3 25 2 N-Ethylformlamide 73 C3H7NO 000627-45-2 9 3 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 4 1-Butanamine, 3-methyl-_____________ 87 C5H13N 000107-85-7 7 Abundance Scan 333 (8.105 min): 6457.D (-) m/z 72.95 100.00% 73

5000 43 TTIOLmmmO/Tu/ 7.80 8.00 8.20 8.40 38.1 1 50 55 67 1 87 103 ' 1 I' 1 ■ ■ i ■" 1 1 1 1 ' ' 1 1 ''' i ■ ■ 1 1 i ''1 1 1 i ’ m/z 43.05 27.45% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73

5000 -PI —er । । । 7.80 8.00 8.20 8.40 m/z 41.05 10.71% 45 15 I 53 59 ।| 88 ' ' i ' '11 1 I 1-1 — m/z—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73 4, , — P 1 —4— '1 | 7.80 8.00 8.20 8.40 5000 m/z 45.05 9.93% 44 58

m/z—> —15...J. — ' ■ 4 — 10 20 30 40 50 60 I ' ' ' ' i ‘ 1 ' ‘ i ‘ 1 1 1 I ' ' 1 1 1 1 1 1 1 1 1 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- 73 7.80 8.00 8.20 8.40 m/z 71.00 6.75%

5000 45

I 1 ' 1 ■ I ■ 2733 39 ■ • ■ I ■ ' I I I I 55 ' I ' 4— 1 1 1 ' I'1 • 1 1 i ■ ■ ■ ■ । ■ i ■ ■ ■ . । ■ T I I I I I I I 1I I 11m T T[ 1 I I I [ m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

6457.D GCMS0412.M Thu Apr 18 09:15:28 2002 Page 1

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