GCMS analysis results for sample AE06457, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1702\6457.D Vial: 15 Acq On : 17 Apr 2002 9:54 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 3 Pyrene, 4-decyl-1,2,3,3a,5a, 6, Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 38.52 1.01 ug/1 93122 Perylene-dl2 37.87 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pyrene, 4-decyl-1,2,3,3a,5a,6,7,8-o 350 C26H38 055493-75-9 27 2 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 23 3 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 22 4 1,1,1,5/7,7,7-Heptamethyl-3,3-bis(t 444 C13H4005Si6 038147-00-1 17

7 Abundance Scan 3646 (38.519 min): 6457.D (-) m/z 73.00 100 .00% 73 147 221 281

5000 355 429 —I I | ! , , I p > , , [ I I I I | I I I I 193 327 |

m/z—> Abundance 44 '' i 50 .L 100 150 200 :250 300 — 254

350 400 38.20 38.40 38.60 38.80 m/z ... 147.00 / 95.36% #49342: Pyrene, 4-decyl-1,2,3,3a,5a,6,7,8-octahydro- 29 221

5000 MAAA 38.20 38.40 38.60 38.80 178 m/z 221.05 91.40% I । । > ■ • ■ । I 22 । ..... 290........ ...... ' I r • mz-> 50 100 150 200 250 300 350 400 Abundance #41682:3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 147 221 "II 73 38.20 38.40 38.60 38.80 I 5000 m/z 281.00 72.30%

m/z-> Abundance T 50 ■ 100 । 117 | / > _j ' l ' 1 1 ' 1 1 ' 150 191

200 279 - 250 #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 300 ’ TT 1—1 350 l 400 77 73 147 38.20 38.40 38.60 38.80 m/z 207.00 38.74% 281 5000 wykat 369 , 207 “T" 249 — 338 1 ' I 1 1 ' 1 I-' 1 1 1 I m/z—> 50 100 150 200 250 300 350 400 38.20 38.40 38.60 38.80

6457.D GCMS0412.M Thu Apr 18 09:15:30 2002 Page 3

NYC-WTC_000039637