GCMS analysis results for sample AE04130, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2202\4130.D Vial: 26 Acq On : 23 Mar 2002 8:43 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.29 0.31 ug/1 34364 1,4-Dichlorobenzene-d4 12.27

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 9 2 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 4 3 2-Acetylthiazole 127 C5H5NOS 024295-03-2 4 4 2-Buten-1-amine, N- butyl-, (Z)- 127 C8H17N __ 062337-87-5 4 Abundance Scan 354 (8.293 min): 4130.D (-) m/ z 43.00 100.00% 43

5000

97 125 ./ .7, ...a 8.00 8.20 8.40 8.60 ............... ................... || ■ • । ■ ■ ■ ■ । ‘ । ■ —H m/z 46.95 15.58% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247:2-Propanone, 1,1,1-trichloro- 43

5000

15 lkuhAuun 8.00 8.20 8.40 ' 8.60 " m/z 124.85 11.95% 35 49 85 97 117 125 ■‘i■■'■i■■■■i■ ■ •■ i ■ ■ ■ *i' ■ ■ ■ i ■ ■ ■ ■ i ■' ■ ■ i T-tV m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance 43 • • I > • > • i • • • i • < • < । ■ 8.00 8.20 8.40 8.60 5000 m/ z 82.85 9.62% 99 127 30 56 86 69 112 ■ ■ i ■ ■ • ■ i ‘ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ I 1 1 ‘ ' i ' ■ 1 ' I ' ' • ' i ' ‘ i ‘ ‘ ‘ i ‘ ‘ I ■ ‘ ‘ ' l ' ‘ ‘ i ' • m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4717:2-Acetylthiazole • ■ i ■ ■ ■ ‘ i ' ■ i ■ ■ ■ ■ i ■ • 43 8.00 8.20 8.40 8.60 m/z 84.85 8.64% 5000 99 58 127 85 112 33 ■ ■ i ■ ■ ■ ■ i ‘ ■ ■ • i ‘ ‘ ‘ i ■ • • ■ i • ■ ***** ‘ ■ f ■ ‘'''I ■ ■ ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 8.00 8.20 8.40 ’ 8.60

4130.D GCMS0308.M Wed Mar 27 10:08:00 2002 Page 2

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