GC/MS analysis results for sample AD30904, Jan 28 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30904.D Vial: 44 Acq On 2 Jan 2002 6:35 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Fluorononane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

7.74 0.88 ug/1 208197 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Fluorononane / 146 C9H19F 000463-18-3 9 2 2-Acetyl-l,4,5, 6-tetrahydropyridine 125 C7H11NO 000000-00-0 4 3 2-Acetylthiazole 127 C5H5NOS 024295-03-2 4 4 1-Hexadecanol 242 C16H340 036653-82-4 4 Abundance Scan 294 (7.741 min): 30904.D (-) m/z 4 .00 100.00% 43

5000 ‘ ‘ i ‘ 1 • ‘ i ■ ' ‘ • l ‘ 11. r . . i t 97 117 125 7.40 7.60 7.80 8.00

m/z-> TIPTT 20 30 37 , 40 +4%.-97il 50 60 70 80 90 I ■ 1 I 1 i I » | I I 1 > | I t 1t 1 > l < | • • 100 110 120 130 m/z 124.85 10.38% Abundance #8922: 1-Fluorononane 43

5000 ‘.d,d,d2n//t/1/7m///0//1/t/558d, 56 7.40 7.60 7.80 8.00 27 70 84 97 m/z 82.95 8.85% 33 m/z-> ■ i • ■ ■ ■ I ''' ‘ ‘ I 20 30 40 "7 — 60 70 ' ’ 80 90 ■ ■ i ■ ■ 1 1 i ■ ' ■ ■ i 1 ■ ■ 1 i ■ ■ ■ ■ i' ■ 100 110 120 130 Abundance #4332: 2-Acetyl-1 4.5.6-tetrahydropyridine i 43 54 82 MMMMAALMAA 7.40 7.60 7.80 8.00 5000- 125 m/z 96.95 8.10%

97 110 I r--r TPBmuutt—ueCrhtir miz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4717: 2-Acetylthiazole ■ ■ i ■ • ■ ■ i • • ' ■ i ■ 1 ■ 1 i ■ ' ■ ' । 43 7.40 7.60 7.80 8.00 m/z 126.90 7.31% 5000 99 58 127 112 85

miz-> 33 • i * • ■ • i ■ • ■ * i < 20 30 40 | • ■ i ‘ ' 50 60 m 70 80 90 ■ I ‘ 100 ‘ ' I 1 110 • • । 120 ■ • I’j ■ ■ ■ 130 ‘ ‘ I 1 ■ ' ' I ' ‘ 1 ' I 1 1 1 1 I ' ' 1 1 I 7.40 7.60 7.80 8.00

30904.D GCMS1126.M Fri Jan 25 11:29:42 2002 Page 2

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