GC/MS analysis results for sample AD30904, Jan 28 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30904.D Vial: 44 Acq On 2 Jan 2002 6:35 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3,4-Dihydroxybenzyl alcohol,tr Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

14.30 1.09 ug/1 318719 Naphthalene-d8 15.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 43 2 N-(Trifluoroacetyl)-0,0‘,0‘ ’-tris(t 481 C19H34F3NO4Si3 000000-00-0 43 3 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 40 4 Benzoic a. d, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 38 Abundance 1 Scan 1009 (14.305 min): 30904.D (-) m/z 73.0,0 100.00% 73

5000 267 355 _>______ / V _______ • j • • • * i . • • . I . . t » i ■ . . • 1 45 103125 154 193 223 , , i 14.00 14.20 14.40 14.60 i । T-r^j-r-r T-pAT1**1" Pi 1*1* fi r T—I‘ 323‘ ’ 1 r m/z 267.00 32.15% 50 100 150 200 250 300 350 400 450 Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsily!) 73 267 5000 179 11 TI 14.00 14.20 14.40 14.60 356 45 147 m/z 355.0 23.61% I |, 209 237 , , 312 j............ 1 1'i rr ■ ‘ i • ■ ■ ■ i • • ‘ ■ i '■ ■ ■ ■ i ■ m/z-> 50 100 150 200 250 300 ' ' 350 400 ' 450 Abundance #58326: N-(Trifluoroacety!)-0.0,0"-tris(trimethylsilyl)no 73 ■ ■ i ■ ■ ■ ■ । ■ ■ ■ • । • ■ ■ ■ । ■ i 355 14.00 14.20 14.40 14.60 5000 m/z 74.00 8.90%

45 I 126147 193 265 376 481 ■ 1 i • ■ ■ ' i • ■ ■ ■ । 1 ■ 1 r ' r 7 i । » I » i j i i-! i pi r-i II” i r T ! 1 I IT miz-> 50 100 150 200 250 300 350 400 450 Abundance #51266: Cyclopentasiloxane, decamethyl- /_____________ ■ ■ i 1 ■ ■ ■ i ■ ■ • • r1-1"1 1 r1 1 1 1 i 73 14.00 14.20 14.40 14.60 m/z 268.00 8.48% 355 267 5000

TI"I hr .27 T J l 323 . 1 » | i i i > j b i I ! | ! T miz-> 50 100 ' ‘ ‘l5o' 200 250 300 350 400 450 14.00 14.20 14.40 14.60

30904.D GCMS1126.M Fri Jan 25 11:29:46 2002 Page 3

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