NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC3101\30705.D Vial: 46
Acq On : 2 Jan 2002 9:30 am Operator: 209 GALOS
Sample : gems scan 12/19a Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
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Peak Number 2 3,4-Dihydroxybenzyl alcohol,tr Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
14.30 1.13 ug/1 333134 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3,4-Dihydroxybenz alcohol,tris(tr 356 C16H3203Si3 068595-79-9 46
2 N- (Trif Luoroacety )-0,0',O"'-tris(t 481 C19H34F3NO4Si3 000000-00-0 38
3 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 33
4 Benzeneethanamine, N-[ (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 32
Abundance Scan 1009 (14.304 mln): 30705.D (-) m/z 73.00 100.00%
73
5000
355267
i » । । n 118s i 41 » »11 । । III’T"*
45 103 133154 193 223 . , 14.00 14.20 14.40 14.60
- TTdnn/r 323
1* A," "I* f, A r. I . — • । ■ • • • । » m/z 267.00 28.63%
miz-> 50 100 150 200 250 300 350 400 450
Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)
73
267
5000 179 T T
14.00 14.20 14.40 14.60
356
45 147 m/z 355.0 22.96%
209 237 , 312
IPIr 200 ' ’250’ ' ।■ 1 1 1 1 1 1 1 1 1
m/z-> 50 100 150 300 350 400 450
Abundance #58326: N-(Trifluoroacetyi)-O.0‘ O"-tris(trimethylsilyl)no
73
355 14.00 14.20 14.40 14.60
5000 m/z 74.00 8.36%
45
, 126147 193 265 | 376 481
I 1 ■ 1 ■ ■ 1 1 1 1 ' ' I 1 1 ' 1 1 ' 1 ' i • ■ ‘ ■ i ‘ ‘ ' i ■ ‘ ' i ' ' ■ ‘ i '
miz-> 50 100 150 200 250 300 350 400 450
Abundance #51266: Cyclopentasiloxane, decamethyl- /_________
*‘I***I1*I***I**
73 14.00 14.20 14.40 14.60
m/z 356.0 7.94%
355
267
5000
207 , 1 323 , _3it
__________ /_________
‘ ‘ i ‘‘ ‘ i ‘ ‘ i ' ' • ■ i ' ■ ■ • I ■ " ‘1 I ’ ' I 'r 11I ‘ 1 1 1 1 1 ] > i • I J » 4 I I | J I I I J! J
m/z-> 50 100 150 200 250 300 350 400 450 14.00 14.20 14.40 14.60
30705.D GCMS1126.M Fri Jan 25 11:27:02 2002 Page 2
NYC-WTC_000018613
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