GCMS calibration table, sample AD31129, Jan 2002

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Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\ JANO 902\31129A.D Vial: 26 Acq On : 10 Jan 2002 3:31 pm Operator: 209 GALOS Sample : gems scan 12/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

14.17 0.28 ug/1 104254 Naphthalene-d8 15.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasilo: .ne, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 3,4 -Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 43 3 N- (Trifluoroacetyl) -0,0',0' '-tris(t 481 C19H34F3NO4Si3 000000-00-0 38 4 Benzeneethanamine, N-[(pentafluorop 475 C21H26F5NO2Si2 055429-85-1 38 Abundance Scan 994 (14.166 min): 31129A.D (-) m/z 73.00 100.00% 73

5000 267 I i 355 . 45 133154 193 237 323 13.80 14.00 14.20 14.40 ‘ • i ’ i’ ■ 14 14, 1* YHih , . 1*** m/z 267.00 31.09% miz-> 50 100 150 200 250 300 350 400 450 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

5000 267 355 .......... M............ 13.80 14.00 14.20 14.40 ' ‘1' m/z 355.0 23.75% , 207 , | 323 | ■ i ' ■ ■ ' i ■ ' ■ ■ i 1 ■ ■ ■ i ‘ '

mz —_ 50 Abundance ■ ■ i ■ ■ ■ ■ i ■ 100 __ 150 149868: 1 i * • 200 250 300 _ p, 1: 350 . 400 450 73

13.80 14.00 14.20 14.40 “ ' 267 5000 179 m/z 356.05 8.67% 356 45 147 209 237 . 312 ' ; ‘ ‘ 1 miz-> 50 100 150 200 250 300 350 400 450 Abundance #58326: N-(Trifluoroacetyl)-O,O',O"-tris(trimethylsilyl)no ■ i ■ ■ ■ ' i ■ 1 ' ■ i ■ • ■ ■ i ■ ■ ■ ■ i ■ 73 13.80 14.00 14.20 14.40 355 m/z 74.00 8.37% 5000

45 1, 126147 193 265 t 376 481 ----- ■ • i ’ ■ — ——— ‘ * I ‘ 1 f ‘ m/z-> 50 100 150 200 250 300 350 400 450 13.80 14.00 14.20 14.40

31129A.D GCMS0103.M Wed Feb 06 09:21:32 2002 Page 3

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