Laboratory document detailing GC/MS calibration data for various compounds and method parameters reviewed on January 9, 2002.
NYC-WTC_000016383–000016391Folder label: “GCMS X 12/24/01 A 1/9/02 2/15/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\JAN0 802\31344.D Vial: 11 Acq On 9 Jan 2002 11:33 pm Operator: 209 GALOS Sample gems scan 12/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 6 11:03 2002 Quant Results File: GCMS0103.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator)
CAe Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.53 152 916103 20.00 ug/1 0.00 10) Naphthalene-d8 15.12 136 3607889 20.00 ug/1 0.00 17) Acenaphthene-diO 20.39 164 1821707 20.00 ug/1 0.00 29) Phenanthrene-diO 24.81 188 2605247 20.00 ug/1 0.00 38) Chrysene-dl2 32.84 240 1513709 20.00 ug/1 0.00 44) Perylene-dl2 36.91 264 879702 20.00 ug/1 0.01
System Monitoring Compounds 37) 2,4-DDD 29.88 235 103092 ( 3.45 g/ mL -0.19 Spiked Amount 5.000 Recovery _ 69.00%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichiorobenzene 0.00 146 0 N.D. ' 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 12.87 77 215 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.19 128 1440 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 20.85 165 296 N.D. 25) Diethylphthalate 21.91 149 683 N.D. 26) 4-Chiorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 9 0 N.D. ' 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 31344.D GCMS0103.M Wed Feb 06 11:04:43 2002 Page 1
NYC-WTC_000016383
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