Laboratory report for DEP sample AD31254 identifying unknown compounds and surrogate recovery results from February 25, 2002.
NYC-WTC_000016480–000016495Folder label: “GCMS X 12/24/01 A 1/9/02 2/15/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\JAN0802\31254.D Vial: 12 Acq On : 10 Jan 2002 12:31 am Operator : 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 6 11:10 2002 Quant Results File: GCMS0103.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.53 152 824485 20.00 ug/1 0.00 10) Naphthalene-d8 15.13 136 3214195 20.00 ug/1 0.00 17) Acenaphthene-diO 20.39 164 1602640 20.00 ug/1 0.00 29) Phenanthrene-diO 24.80 188 2238440 20.00 ug/1 0.00 38) Chrysene-dl2 32.84 240 1290681 20.00 ug/1 0.00 44) Perylene-dl2 36.90 264 759683 20.00 ug/1 0.00
System Monitoring Compounds 37) 2,4-DDD 29.89 235 95921 3.73 ug/mL -0.18 Spiked Amount 5.000 Recovery = 74.60%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine. 5.14 74 465 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. s 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.18 128 1375 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 20.50 153 189 N.D. 24) 2,4-Dinitrotoluene 20.65 165 686 N.D. 25) Diethylphthalate 21.92 149 1346 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 31254.D GCMS0103.M Wed Feb 06 11:11:20 2002 Page 1
NYC-WTC_000016482
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Laboratory report for DEP sample AD31253 identifying unknown compounds and surrogate recovery results from February 25, 2002.
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1 shared topics · Same agency, volume and box · similarity 0.997
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