Laboratory report for DEP sample AD31251 identifying unknown compounds and surrogate recovery results from February 25, 2002.
NYC-WTC_000016461–000016479Folder label: “GCMS X 12/24/01 A 1/9/02 2/15/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\JAN0 802\31251.D Vial: 16 Acq On : 10 Jan 2002 4:26 am Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 6 10:01 2002 Quant Results File: GCMS0103.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.53 152 907810 20.00 ug/1 0.00 10) Naphthalene-d8 15.13 136 3531183 20.00 ug/1 0.00 17) Acenaphthene-diO 20.40 164 1800400 20.00 ug/1 0.00 29) Phenanthrene-diO 24.81 188 2556966 20.00 ug/1 0.00 3 8) Chrysene-dl2 32.84 240 1524455 20.00 ug/1 0.00 44) Perylene-dl2 36.90 264 867872 20.00 ug/1 0.00
System Monitoring Compounds 37) 2,4-DDD 29.89 235 118605 4.04 ug/mL -0.18 Spiked Amount 5.000 Recovery = 80.80%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.14 74 573 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 13.36 82 170 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.18 128 1269 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 20.84 165 183 N.D. 25) Diethylphthalate 21.91 149 1494 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 2 7) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 31251.D GCMS0103.M Wed Feb 06 11:12:41 2002 Page 1
NYC-WTC_000016463
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Laboratory report for DEP sample AD31253 identifying unknown compounds and surrogate recovery results from February 25, 2002.
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1 shared topics · Same agency, volume and box · similarity 0.997
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1 shared topics · Same agency, volume and box · similarity 0.997
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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AD31461 conducted on February 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
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