NYC-WTC_000018005
Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.
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GCMS analysis summary, sample AD27288, Dec 2001
Machine-extracted title · confidence 100%GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
NYC-WTC_000016096–000016117Folder label: “GCMS X 12/26/01 A 1/15-1/16/02”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\JAN0 802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 16:30 2002 Quant Results File: GCMS0103.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.53 152 802064 20.00 ug/1 0.00 10) Naphthalene-d8 15.13 136 3102307 20.00 ug/1 0.00 17) Acenaphthene-diO 20.39 164 1526223 20.00 ug/1 0.00 29) Phenanthrene-diO 24.80 188 2301677 20.00 ug/1 0.00 38) Chrysene-dl2 32.84 240 1441482 20.00 ug/1 0.00 44) Perylene-dl2 36.90 264 847965 20.00 ug/1 0.00
System Monitoring Compounds 37) 2,4-DDD 29.89 235 131166 4.96 ug/mL -0.18 Spiked Amount 5.000 Recovery = 99.20%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.22 74 295 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.18 128 645 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.20 162 657 N.D. 20) Dimethylphthalate 20.12 163 514 N.D. 21) 2,6-Dinitrotoluene 20.13 165 193 N.D. 2 2) Acenaphthylene 20.07 152 396 N.D. 23) Ac enapht hene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 20.86 165 1826 N.D. 25) Diethylphthalate 21.92 149 1108 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 27288.D GCMS1126.M Mon Feb 04 14:36:55 2002 Page 1
NYC-WTC_000016098
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