NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\l\DATA\JAN0802\27288.D Vial: 26
Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS
Sample gems scan 12/20a Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Jan 9 16:30 2002 Quant Results File: GCMS0103.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Mon Jan 07 10:31:02 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.53 152 802064 20.00 ug/1 0.00
10) Naphthalene-d8 15.13 136 3102307 20.00 ug/1 0.00
17) Acenaphthene-diO 20.39 164 1526223 20.00 ug/1 0.00
29) Phenanthrene-diO 24.80 188 2301677 20.00 ug/1 0.00
38) Chrysene-dl2 32.84 240 1441482 20.00 ug/1 0.00
44) Perylene-dl2 36.90 264 847965 20.00 ug/1 0.00
System Monitoring Compounds
37) 2,4-DDD 29.89 235 131166 4.96 ug/mL -0.18
Spiked Amount 5.000 Recovery = 99.20%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.22 74 295 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) 1sophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichiorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.18 128 645 N.D.
16) Hexachiorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 18.20 162 657 N.D.
20) Dimethylphthalate 20.12 163 514 N.D.
21) 2,6-Dinitrotoluene 20.13 165 193 N.D.
22) Acenaphthylene 20.07 152 396 N.D.
2 3) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 20.86 165 1826 N.D.
25) Diethylphthalate 21.92 149 1108 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
2 8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
27288.D GCMS0103.M Thu Jan 10 09:32:51 2002 Page 1
NYC-WTC_000018008
OCR can misread numbers and units. Confirm readings against the page image before using them.