NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C: \HPCHEM\1\DATA\ JAN0802\31255 .D Vial: 9
Acq On 9 Jan 2002 9:35 pm Operator: 209 GALOS
Sample gems scan 12/24 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Feb 6 10:03 2002 Quant Results File: GCMS0103.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Thu Dec 13 14:40:46 2001
Response via : Initial Calibration
DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) l,4-Dichlorobenzene-d4 11.53 152 858927 20.00 ug/1 0.00
10) Naphthalene-d8 15.13 136 3466709 20.00 ug/1 0.00
17) Acenaphthene-diO 20.40 164 1765499 20.00 ug/1 0.00
29) Phenanthrene-diO 24.81 188 2499005 20.00 ug/1 0.00
38) Chrysene-dl2 32.84 240 1469242 20.00 ug/1 0.00
44) Perylene-dl2 36.90 264 851932 20.00 ug/1 0.00
System Monitoring Compounds
37) 2,4-DDD 29.89 235 106030 3.70 ug/mL -0.18
Spiked Amount 5.000 Recovery = 74.00%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.16 74 302 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichiorobenzene 0.00 146 0 N.D.
7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) 1sophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichiorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.18 128 178.6 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 19.96 165 240 N.D.
22) Ac enapht hylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 21.92 149 1620 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
31255.D GCMS0103.M Wed Feb 06 11:08:26 2002 Page 1
NYC-WTC_000016425
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