Laboratory report for DEP sample AD31253 identifying unknown compounds and surrogate recovery results from February 25, 2002.
NYC-WTC_000016442–000016460Folder label: “GCMS X 12/24/01 A 1/9/02 2/15/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C: \HPCHEM\ 1 \DATA\JANO 802\31253.D Vial: 10 Acq On 9 Jan 2002 10:34 pm Operator: 209 GALOS Sample gems scan 12/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 6 11:09 2002 Quant Results File: GCMS0103.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) l,4-Dichlorobenzene-d4 11.52 152 866504 20.00 ug/1 0.00 10) Naphthalene-d8 15.12 136 3391749 20.00 ug/1 0.00 17) Acenaphthene-diO 20.39 164 1705627 20.00 ug/1 0.00 29) Phenanthrene-diO 24.81 188 2393839 20.00 ug/1 0.00 38) Chrysene-dl2 32.84 240 1430776 20.00 ug/1 0.00 44) Perylene-dl2 36.91 264 852745 20.00 ug/1 0.01
System Monitoring Compounds 37) 2,4-DDD 29.88 235 106895 3.89 ug/mL -0.19 Spiked Amount 5.000 Recovery = 77.80%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.15 74 401 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. ' 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(l-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.18 128 1212 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 19.80 163 252 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D,. 24) 2,4-Dinitrotoluene 20.78 165 203 N.D. 25) Diethylphthalate 21.92 149 1753 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 31253.D GCMS0103.M Wed Feb 06 11:09:44 2002 Page 1
NYC-WTC_000016444
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